• 专利标题:   Chemical method for preparing graphene used for industrialized application, involves preparing graphene oxide, adding oxalic acid crystal to resulting suspension liquid followed by heating, stirring, reacting, warming, washing and drying.
  • 专利号:   CN102219210-A, CN102219210-B
  • 发明人:   CUI X, SONG P, SUN M, ZHANG X
  • 专利权人:   UNIV FUDAN
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102219210-A 19 Oct 2011 C01B-031/04 201220 Pages: 7 Chinese
  • 申请详细信息:   CN102219210-A CN10089147 11 Apr 2011
  • 优先权号:   CN10089147

▎ 摘  要

NOVELTY - A graphene preparing method involves preparing graphene oxide by Hummer's oxidation process by utilizing graphite powder as raw material. Oxalic acid crystal is added to resulting suspension liquid heated at 65-95 degrees C, stirred under magnetic force and reacted for 4-20 hours. The obtained product is warmed up to temperature of 140-160 degrees C. Excess oxalic acid is removed, and the resulting product is washed and dried to obtain graphene product. USE - Chemical method for preparing graphene that is utilized for industrialized application. ADVANTAGE - The method enables preparing graphene with reduced toxicity and high purity in an inexpensive manner. DESCRIPTION OF DRAWING(S) - The drawing shows a graph illustrating infrared spectrum result of the graphene.