• 专利标题:   Preparing hydrophobic graphene film by preparing graphene dispersion and nanoparticle dispersion, mixing, depositing on support, drying, soaking in hydrophobic modifier solution using hydrophobic modifier, water and ethanol, and treating.
  • 专利号:   CN111450711-A
  • 发明人:   LIU G, ZHANG M, JIN W
  • 专利权人:   UNIV NANJING TECHNOLOGY
  • 国际专利分类:   B01D061/36, B01D067/00, B01D069/02, B01D069/10, B01D071/02, C01B032/182, C01B032/194, C02F001/44, C02F103/08
  • 专利详细信息:   CN111450711-A 28 Jul 2020 B01D-067/00 202066 Pages: 10 Chinese
  • 申请详细信息:   CN111450711-A CN10439034 22 May 2020
  • 优先权号:   CN10439034

▎ 摘  要

NOVELTY - Method for preparing hydrophobic graphene film involves (i) adding graphene oxide to water, stirring and ultrasonically treating to obtain a uniformly dispersed graphene dispersion, (ii) adding nanoparticles into water, stirring and ultrasonically treating to obtain a uniformly dispersed nanoparticle dispersion, (iii) mixing hydrophobic modifier, water, and ethanol, and uniformly stirring to obtain a hydrolyzed hydrophobic modifier solution, (iv) adding the nanoparticle dispersion to the graphene dispersion, uniformly stirring, depositing on support by vacuum filtration to form a nano-film and drying to obtain rough graphene film, and (v) soaking the prepared film in the hydrophobic modifier solution for a period of time, cleaning the surface of the film, and forming the hydrophobic graphene film by heat treatment. USE - The method is useful for preparing hydrophobic graphene film. ADVANTAGE - The method enhances interlayer pores and surface roughness of the graphene film by intercalated nanoparticles and treats with long-chain alkanes to obtain the hydrophobic graphene film, improves the surface roughness and hydrophobicity of the graphene oxide, is simple and convenient to realize the effective desalination and anti-pollution performance of the hydrophobic graphene film in the membrane distillation process.