• 专利标题:   Preparation of borax buffer system graphene/carbon paper gas electrode involves flattening hydrophobic carbon paper, controlling water contact angle, ultrasonic dispersing graphene oxide flakes in borax buffer, and reacting.
  • 专利号:   CN107026274-A
  • 发明人:   ZHANG P, HONG J, LI Y, ZHANG J, FU F, WANG Z
  • 专利权人:   UNIV CHINA GEOSCIENCES WUHAN
  • 国际专利分类:   H01M012/06, H01M004/88, H01M004/96
  • 专利详细信息:   CN107026274-A 08 Aug 2017 H01M-004/96 201760 Pages: 14 Chinese
  • 申请详细信息:   CN107026274-A CN10344310 16 May 2017
  • 优先权号:   CN10344310

▎ 摘  要

NOVELTY - Preparation of borax buffer system graphene/carbon paper gas electrode involves flattening hydrophobic carbon paper to 25-34 mu m thickness, controlling water contact angle at 90-140 degrees , ultrasonic dispersing graphene oxide flakes in borax buffer, assembling electrophoresis cell using hydrophobic carbon paper as positive electrode, platinum as negative electrode and graphene oxide as electrolytic solution, performing decarboxylation reaction, controlling cell voltage with direct current power supply, real-time monitoring electrolyte conductivity, and stirring to obtain reduced graphene oxide. USE - Method for preparing borax buffer system graphene/carbon paper gas electrode (claimed). ADVANTAGE - The electrode is environment-friendly, stable, and has improved charging/discharging cycle. The method is simple, and easy. DETAILED DESCRIPTION - Preparation of borax buffer system graphene/carbon paper gas electrode comprises flattening hydrophobic carbon paper to 25-34 mu m thickness, controlling water contact angle at 90-140 degrees , ultrasonic dispersing graphene oxide flakes in borax buffer, assembling electrophoresis cell using hydrophobic carbon paper as positive electrode, platinum as negative electrode and graphene oxide as electrolytic solution, performing decarboxylation reaction, controlling cell voltage with direct current power supply, real-time monitoring electrolyte conductivity, stirring to obtain reduced graphene oxide, removing carbon paper electrode, washing with secondary distilled water and 0.1 mol/dm3 barium chloride solution, precipitating, and drying.