• 专利标题:   Preparation of graphene glass involves cleaning glass substrate, spin coating, concentrating copper salt solution, spin coating glass substrate of copper salt solution in chemical gas phase deposition device, heating, and filling hydrogen.
  • 专利号:   CN107311466-A
  • 发明人:   LIU Z, QU Y
  • 专利权人:   UNIV PEKING
  • 国际专利分类:   C03C017/22
  • 专利详细信息:   CN107311466-A 03 Nov 2017 C03C-017/22 201777 Pages: 8 Chinese
  • 申请详细信息:   CN107311466-A CN10328535 11 May 2017
  • 优先权号:   CN10328535

▎ 摘  要

NOVELTY - Preparation of graphene glass involves cleaning glass substrate; spin coating layer of copper salt solution on resistant at high temperature glass substrate, and concentrating copper salt solution; spin coating glass substrate of copper salt solution in chemical gas phase deposition device, and heating to 1000-1100 degrees C under protection of inert gas; annealing at 1000-1100 degrees C, filling hydrogen and argon, and reducing copper salt; and keeping at 1000-1100 degrees C, introducing carbon source and hydrogen, chemical vapor deposition reaction in reaction chamber, closing carbon source, and cooling. USE - Method for preparing graphene glass (claimed). DETAILED DESCRIPTION - Preparation of graphene glass comprises cleaning glass substrate; spin coating layer of copper salt solution on resistant at high temperature glass substrate, and concentrating copper salt solution; spin coating glass substrate of copper salt solution in chemical gas phase deposition device, and heating to 1000-1100 degrees C under protection of inert gas; annealing at 1000-1100 degrees C, filling hydrogen and argon, and reducing copper salt; and keeping at 1000-1100 degrees C, introducing carbon source and hydrogen, chemical vapor deposition reaction in reaction chamber, closing carbon source, and cooling to room temperature.