• 专利标题:   In-line polymerization-solution phase-based preparation of oxidized graphene/polybutylene succinate composite material, involves dispersing graphene oxide and polybutylene succinate in solvent, and dissolving polybutylene succinate.
  • 专利号:   CN106243644-A, CN106243644-B
  • 发明人:   HUANG J, CUI C
  • 专利权人:   UNIV NINGDE NORMAL, UNIV NINGDE NORMAL
  • 国际专利分类:   B29B007/72, C08K003/04, C08L067/02
  • 专利详细信息:   CN106243644-A 21 Dec 2016 C08L-067/02 201724 Pages: 8 Chinese
  • 申请详细信息:   CN106243644-A CN10705549 23 Aug 2016
  • 优先权号:   CN10705549

▎ 摘  要

NOVELTY - The in-line polymerization-solution phase-based preparation method of oxidized graphene/polybutylene succinate composite material involves (i) uniformly dispersing graphene oxide and polybutylene succinate in solvent (a), and dissolving polybutylene succinate to form a mixed solution, (ii) pouring solvent (b) into mixed solution, precipitating polybutylene succinate, (iii) removing the solvent (a) and solvent (b) in product, (iv) mixing the product with catalyst in a two-roll mill, and placing in a two-roll mill at 120 degrees C. USE - In-line polymerization-solution phase-based preparation of oxidized graphene/polybutylene succinate composite material (claimed). DETAILED DESCRIPTION - The in-line polymerization-solution phase-based preparation method of oxidized graphene/polybutylene succinate composite material involves (i) uniformly dispersing graphene oxide and polybutylene succinate in solvent (a), and dissolving polybutylene succinate to form a mixed solution, (ii) pouring solvent (b) into mixed solution, precipitating polybutylene succinate, where the polybutylene succinate is insoluble or sparingly soluble in solvent (b), (iii) removing the solvent (a) and solvent (b) in product, (iv) mixing the product with catalyst in a two-roll mill at 110 degrees C, placing in a two-roll mill at 120 degrees C, reducing the roller temperature to 90 degrees C, until the sample surface is smooth and uniform.