• 专利标题:   Graphene preparation involves mixing concentrated sulfuric acid and concentrated nitric acid in reactor to obtain mixed acid solution, and then adding graphite to the mixed acid solution to obtain a mixture.
  • 专利号:   CN103936000-A, CN103936000-B
  • 发明人:   JIN C, YANG X
  • 专利权人:   SUZHOU SDIK NEW MATERIAL TECHNOLOGY STOC, SUZHOU SIDIKE NEW MATERIALS SCI TECHNO
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103936000-A 23 Jul 2014 C01B-031/04 201468 Pages: 6 Chinese
  • 申请详细信息:   CN103936000-A CN10201727 14 May 2014
  • 优先权号:   CN10201727

▎ 摘  要

NOVELTY - Graphene preparation involves mixing concentrated sulfuric acid and concentrated nitric acid in reactor to obtain mixed acid solution, and then adding graphite to the mixed acid solution to obtain a mixture. The obtained mixture is stirred, and then potassium chlorate is added to the stirred mixture. The mixture is processed in nitrogen atmosphere. The mixture is washed with deionized water, and then further washed with potassium hydroxide and acidic aqueous solution. The washed material is dried in presence of vacuum at 160-220 degrees C for 4-24 hours. USE - Method for preparing graphene (claimed). DETAILED DESCRIPTION - Graphene preparation involves mixing concentrated sulfuric acid and concentrated nitric acid in reactor to obtain mixed acid solution, and then adding graphite to the mixed acid solution to obtain a mixture. The obtained mixture is stirred, and then potassium chlorate is added to the stirred mixture. The mixture is processed in nitrogen atmosphere. The mixture is washed with deionized water, and then further washed with potassium hydroxide and acidic aqueous solution. The washed material is dried in presence of vacuum at 160-220 degrees C for 4-24 hours. Solid graphite oxide is added to the dried product, and then stirred at 100 degrees C for 5-48 hours. The stirred material is dried in presence of vacuum to obtain the desired product.