• 专利标题:   Producing a graphite powder useful for preparing graphene, comprises e.g. taking natural crystalline flake graphite or artificial graphite, adding oxidant for oxidation reaction to prepare oxidized graphite, and adding intercalation agent.
  • 专利号:   CN112456478-A
  • 发明人:   XIANG X
  • 专利权人:   XIANG X
  • 国际专利分类:   B01F007/04, C01B032/19, C01B032/21
  • 专利详细信息:   CN112456478-A 09 Mar 2021 C01B-032/19 202125 Pages: 16 Chinese
  • 申请详细信息:   CN112456478-A CN11415070 07 Dec 2020
  • 优先权号:   CN11415070

▎ 摘  要

NOVELTY - Producing a graphite powder comprises e.g. taking natural crystalline flake graphite or artificial graphite as raw material, adding oxidant for oxidation reaction to prepare oxidized graphite, then adding intercalation agent for intercalation reaction, after finishing intercalation reaction, filtering the reaction liquid, washing the filtered solid to neutral, drying, obtaining the dried intercalated graphite, using the grinding device to grind and sieve the dried intercalated graphite, obtaining expandable graphite, crushing the expandable graphite by a crusher, then using the stirring device to stir the crushed expandable graphite uniformly, where the stirring device comprises a bottom plate, the top of the bottom plate is fixedly connected with a bottom frame, and the right side of the top part of the bottom frame is fixedly connected with an extending frame, and the inner part of the extending frame is fixed with a stirring tank. USE - The graphite powder is useful for preparing graphene (claimed). ADVANTAGE - The method: provides the left side of the top part of the bottom plate with a receiving mechanism; uses the third motor to provide power through the annular rack; uses big gear and small gear transmission power, which can drive the material collecting cylinder uniformly rotate, and matched with the hydraulic rod; uses a mounting plate and a cleaning brush, which is convenient to clean the inner wall of the material receiving cylinder after taking the material. DETAILED DESCRIPTION - Producing a graphite powder comprises (i) taking natural crystalline flake graphite or artificial graphite as raw material, adding oxidant for oxidation reaction to prepare oxidized graphite, then adding intercalation agent for intercalation reaction, after finishing intercalation reaction, filtering the reaction liquid; washing the filtered solid to neutral; drying, obtaining the dried intercalated graphite; (ii) using the grinding device to grind and sieve the dried intercalated graphite prepared in the step (i), obtaining expandable graphite; (iii) crushing the expandable graphite obtained in the step (ii) by a crusher, then using the stirring device to stir the crushed expandable graphite uniformly, where in the step (iii), the stirring device comprises a bottom plate, the top of the bottom plate is fixedly connected with a bottom frame, and the right side of the top part of the bottom frame is fixedly connected with an extending frame, the inner part of the extending frame is fixed with a stirring tank and the top of the stirring tank is connected and fixed with a first feeding hopper between the bottom frame and the stirring tank is provided with a stirring mechanism, the front and back two sides of the right side of the top of the bottom plate are fixedly connected with a baffle between the two baffle plates is clamped with a switching box. The two sides of the switching box are fixedly installed with a handle, and the inner part of the switching box is provided with a filtering mechanism. The discharging hopper is located right above the switching box, the top part of the bottom plate and the bottom frame are fixedly connected with a supporting frame, the top part of the two supporting frames are fixedly connected with a fine cylinder, and the top of the fine cylinder is connected and fixed with a second feeding hopper, the inner part of the fine cylinder is provided with an optimizing mechanism, and the left side of the fine cylinder is provided with a discharging control mechanism and the left side of the top part of the bottom plate is provided with a receiving mechanism.