• 专利标题:   Preparing lithium titanate/graphene nano-composite material involves dissolving oxidized graphite into deionized water, ultrasonic dispersing to obtain oxidized graphite sol, and stirring oxidized graphite sol.
  • 专利号:   CN106966387-A, CN106966387-B
  • 发明人:   SHU D, MENG T, YI F, CHENG H, HUANG Y, GAO A, ZHANG F
  • 专利权人:   UNIV SOUTH CHINA NORMAL, UNIV SOUTH CHINA NORMAL
  • 国际专利分类:   C01B032/192, C01G023/00, H01G011/06, H01G011/50, H01M004/36, H01M004/58, H01M004/62
  • 专利详细信息:   CN106966387-A 21 Jul 2017 C01B-032/192 201767 Pages: 9 Chinese
  • 申请详细信息:   CN106966387-A CN10283231 26 Apr 2017
  • 优先权号:   CN10283231

▎ 摘  要

NOVELTY - Preparing lithium titanate/graphene nano-composite material involves dissolving oxidized graphite into deionized water, ultrasonic dispersing to obtain oxidized graphite sol. The obtained oxidized graphite sol is stirred, and added cyclodextrin solution to obtain beta -cyclodextrin-oxidized graphite supramolecular sol-gel A. The titanium dioxide suspension is added into sol-gel A, and added ammonia to adjusted pH, irradiated with ultraviolet light to obtain titanium dioxide beta -cyclodextrin-oxidized graphite supramolecular system sol. USE - Method for preparing lithium titanate/graphene nano-composite material (claimed). ADVANTAGE - The method enables to prepare lithium titanate/graphene nano-composite material which has improves conductive efficiency of the lithium titanate. DETAILED DESCRIPTION - Preparing lithium titanate/graphene nano-composite material involves dissolving oxidized graphite into deionized water, ultrasonic dispersing to obtain oxidized graphite sol. The obtained oxidized graphite sol is stirred, and added cyclodextrin solution to obtain beta -cyclodextrin-oxidized graphite supramolecular sol-gel A. The titanium dioxide suspension is added into sol-gel A, and added ammonia to adjusted pH, irradiated with ultraviolet light to obtain titanium dioxide beta -cyclodextrin-oxidized graphite supramolecular system sol, and obtain sol is centrifuged to obtain concentrated liquid and freeze-dried to obtain solid B. The lithium source and resulted solid B are transferred to ball mill for ball milling, resulted powder is calcined in inert gas atmosphere to obtain final product.