• 专利标题:   Production of polyaniline-based europium oxide/graphene conductive thin film involves preparing graphene/europium oxide dispersion liquid, dispersing with aniline, adding hydrochloric acid, cooling, reacting, filtering, washing, and drying.
  • 专利号:   CN105778132-A
  • 发明人:   HE W, YU X, ZHANG L, ZHAO L
  • 专利权人:   UNIV SHENYANG CHEM TECHNOLOGY
  • 国际专利分类:   C08G073/02, C08J005/18, C08K003/04, C08K003/22, C08K009/02, C08L079/02
  • 专利详细信息:   CN105778132-A 20 Jul 2016 C08J-005/18 201674 Pages: 11 Chinese
  • 申请详细信息:   CN105778132-A CN10197064 31 Mar 2016
  • 优先权号:   CN10197064

▎ 摘  要

NOVELTY - Production of polyaniline-based europium oxide/graphene conductive thin film comprises preparing graphene oxide; preparing graphene-based europium oxide; taking 1 pt. wt. graphene/europium oxide dispersion liquid and mixing with 50 pts. wt. 1 mol/L aniline; ultrasonically dispersing at 20-25 degrees C for 30 minutes, adding 30 pts. wt. 1 mol/L hydrochloric acid, and stirring under ice bath condition; cooling to 0 degrees C and mixing with ammonium persulfate; reacting for 0-5 hours at 5-24 degrees C and stirring at 20-25 degrees C for 12 hours; and filtering, washing with ethanol and deionized water, and vacuum drying. USE - Method for producing polyaniline-based europium oxide/graphene conductive thin film (claimed). ADVANTAGE - The film has superior conductivity performance and good rare earth metal characteristics and achieves photoelectric optical switch function. DETAILED DESCRIPTION - Production of polyaniline-based europium oxide/graphene conductive thin film comprises preparing graphene oxide; preparing graphene-based europium oxide; taking 1 pt. wt. graphene/europium oxide dispersion liquid and mixing with 50 pts. wt. 1 mol/L aniline; ultrasonically dispersing at 20-25 degrees C for 30 minutes, adding 30 pts. wt. 1 mol/L hydrochloric acid, and stirring under ice bath condition; cooling to 0 degrees C and mixing with ammonium persulfate; reacting for 0-5 hours at 5-24 degrees C and stirring at 20-25 degrees C for 12 hours; and filtering, washing with ethanol and deionized water, and vacuum drying at 60-80 degrees C for 1- 24 hours.