• 专利标题:   Preparing graphene composite benzoxazine bipolar plate comprises adding graphene oxide into deionized water, adding hydrazine hydrate solution, adding reduced graphene oxide into m-cresol, adding paraformaldehyde and aniline, and mixing graphite filler with graphene-benzoxazine resin mixed powder.
  • 专利号:   CN115566218-A
  • 发明人:   SHEN J, SHANG Z, ZHU W, XIE J
  • 专利权人:   HAIZHUO DONGLI QINGDAO ENERGY TECHNOLOGY
  • 国际专利分类:   C01B032/184, C01B032/194, H01M008/0202, H01M008/0223
  • 专利详细信息:   CN115566218-A 03 Jan 2023 H01M-008/0223 202312 Chinese
  • 申请详细信息:   CN115566218-A CN11331042 28 Oct 2022
  • 优先权号:   CN11331042

▎ 摘  要

NOVELTY - Preparing graphene composite benzoxazine bipolar plate comprises (i) freezing the graphene oxide, adding into deionized water, adding hydrazine hydrate solution after stirring for 1-2 hours, adjusting the pH to 9.5-10.5, washing after stirring for 3-5 hours, and freeze-drying to obtain the reduced graphene oxide, (ii) adding reduced graphene oxide into m-cresol and ultrasonically dispersing for 0.5-1 hours, adding paraformaldehyde and aniline, adding into vacuum oven at 90-120℃ for 0.5-1 hour, filtering the mixture and washing to obtain graphene-benzoxazine resin mixed powder, (iii) mixing the graphite filler with the graphene-benzoxazine resin mixed powder, and stirring mechanically for 1-3 hours, and (iv) placing powder in a molding cavity, molding, solidifying at 150-300℃ for 0.5-1 hour. USE - The method is useful for preparing graphene composite benzoxazine bipolar plate. ADVANTAGE - The method enables the graphene to play a stable role in the benzoxazine, and the prepared bipolar plate graphene composite benzoxazine bipolar plate has the characteristics of high strength, high heat resistance and high conductivity. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for graphene composite benzoxazine bipolar plate, prepared by the above method.