• 专利标题:   Preparing graphene/graphene nano belt/nickel disulfide composite aerogel used in electrode materials for supercapacitors, e.g. comprises preparing graphene oxide nano belt, graphene oxide and mixing with hexadecyl trimethyl ammonium bromide.
  • 专利号:   CN110759340-A
  • 发明人:   ZHENG Y, ZHOU J
  • 专利权人:   FUJIAN CHENQI NEW MATERIAL TECHNOLOGY CO
  • 国际专利分类:   B01J013/00, C01B032/198, C01G053/11, H01G011/24, H01G011/30, H01G011/36, H01G011/86
  • 专利详细信息:   CN110759340-A 07 Feb 2020 C01B-032/198 202018 Pages: 6 Chinese
  • 申请详细信息:   CN110759340-A CN11017474 24 Oct 2019
  • 优先权号:   CN11017474

▎ 摘  要

NOVELTY - Preparing graphene/graphene nano belt/nickel disulfide composite aerogel comprises (i) preparing graphene oxide nano belt, (ii) preparing graphene oxide, (iii) mixing 0.1 g graphene oxide nano belt obtained in the step (i), 0.1 g graphene oxide obtained in the step (ii), and 1 g hexadecyl trimethyl ammonium bromide, then adding 100 ml deionized water, and ultrasonically treating to obtain mixed solution, (iv) adding 0.6 g thiophene, 50 ml n-octane and 0.4 g nickel nitrate to the mixture obtained in the step (iii), hydrothermally reacting at 165-180 degrees C for 4-6 hours to obtain hydrogel, (v) placing the hydrogel obtained in the step (iv) into a potassium nitrate solution, performing secondary hydrothermal reaction at 120-130 degrees C for 2-3 hours, cooling to room temperature, filtering, washing and freeze-drying, and (vi) thermally cracking the product obtained after freeze drying in the step (v) in an argon atmosphere to obtain the product. USE - The graphene/graphene nano belt/nickel disulfide composite aerogel is useful in electrode materials for supercapacitors. ADVANTAGE - The method: improves the electrochemical performance of the graphene/graphene nano belt/nickel disulfide composite aerogel. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for using the graphene/graphene nano belt/nickel disulfide composite aerogel, comprising adding graphene/graphene nano belt/nickel disulfide composite aerogel, acetylene black, and polytetrafluoroethylene emulsion into the same weighing bottle in a mass ratio of 90:5:5, stirring and mixing uniformly, blowing the sample to a paste with an electric blower, using nickel foam as the current collector, coating the paste material on nickel foam, and vacuum-drying at 120 degrees C for 24 hours to obtain the required electrode.