• 专利标题:   Preparing graphene/montmorillonite composite porous thin film used in adsorption field, by adding oxidized graphite powder and montmorillonite powder into solvent, ultrasonically dispersing, evaporating, drying, heat treating, and cooling.
  • 专利号:   CN106517993-A, CN106517993-B
  • 发明人:   SHEN B, ZHENG W, LI Y, ZHANG L
  • 专利权人:   NINGBO INST MATERIALS TECHNOLOGY ENG C
  • 国际专利分类:   C04B030/00, C04B038/06, C01B032/184
  • 专利详细信息:   CN106517993-A 22 Mar 2017 C04B-030/00 201727 Pages: 9 Chinese
  • 申请详细信息:   CN106517993-A CN10905133 18 Oct 2016
  • 优先权号:   CN10905133

▎ 摘  要

NOVELTY - A graphene/montmorillonite composite porous thin film is prepared by adding oxidized graphite powder and montmorillonite powder into solvent, ultrasonically dispersing to obtain graphene oxide/montmorillonite composite dispersion; pouring into evaporating dish, evaporating at a temperature of 40-90 degrees C to form a film, drying to obtain graphene oxide/montmorillonite composite thin film having layered structure; subjecting into heat treatment, and then cooling to obtain the graphene/montmorillonite composite porous thin film. USE - Method for preparing graphene/montmorillonite composite porous thin film used in adsorption field. ADVANTAGE - The method can prepare graphene/montmorillonite composite porous thin film having two sides with different structure. The thin film has evaporation surface with flat crack-shaped structure, and contact surface with loose worm-like structure which can facilitate rapid absorption of liquid. The presence of montmorillonite can improve the final graphene/montmorillonite composite porous film burning loss resisting performance. Further, the method has simple steps, is convenient to operate, and provides a new idea for preparing graphene-based composite porous thin film having excellent performance and great application prospect in adsorption field. DETAILED DESCRIPTION - A graphene/montmorillonite composite porous thin film is prepared by: (1) adding oxidized graphite powder and montmorillonite powder into solvent based on an oxidized graphite powder/montmorillonite powder/solvent weight ratio of 1:(0.01-2):(50-1000), ultrasonically dispersing to obtain graphene oxide/montmorillonite composite dispersion; (2) pouring the graphene oxide/montmorillonite composite dispersion into evaporating dish, evaporating at a temperature of 40-90 degrees C to form a film, drying to obtain graphene oxide/montmorillonite composite thin film having layered structure and thickness of 5-100 mu m; and (3) contacting the graphene oxide/montmorillonite composite thin film with flame in air to carry out heat treatment, and then cooling to obtain the graphene/montmorillonite composite porous thin film. An INDEPENDENT CLAIM is included for the prepared graphene/montmorillonite composite porous thin film.