• 专利标题:   Preparing foldable graphene film involves preparing graphite oxide suspension, adding reducing agent to graphite oxide suspension and uniformly stirring mixture to obtain mixed solution of graphite oxide.
  • 专利号:   CN105967172-A, CN105967172-B
  • 发明人:   YE X, JIA C, ZHOU Q, WAN Z
  • 专利权人:   UNIV CHINA ELECTRONIC SCI TECHNOLOGY, UNIV CHINA ELECTRONIC SCI TECHNOLOGY
  • 国际专利分类:   C01B031/04, C01B032/184
  • 专利详细信息:   CN105967172-A 28 Sep 2016 C01B-031/04 201709 Chinese
  • 申请详细信息:   CN105967172-A CN10298346 06 May 2016
  • 优先权号:   CN10298346

▎ 摘  要

NOVELTY - Preparing foldable graphene film involves preparing an graphite oxide suspension having a mass concentration of 0.1-150 mg/mL, adding a reducing agent to the graphite oxide suspension and uniformly stirring the mixture to obtain a mixed solution of the graphite oxide and the reducing agent, where the concentration of the reducing agent is 47-58 wt.% and the mass ratio of the reducing agent to the oxidized graphite is 6-27. USE - Method for preparing foldable graphene film (claimed). ADVANTAGE - The method enables to prepare foldable graphene film, that has enlarged specific surface area, while forming a loose multilayer structure inside the graphene film, which reduces the agglomeration of the graphene and improves the quality of the graphene film. DETAILED DESCRIPTION - Preparing foldable graphene film involves preparing an graphite oxide suspension having a mass concentration of 0.1-150 mg/mL, adding a reducing agent to the graphite oxide suspension and uniformly stirring the mixture to obtain a mixed solution of the graphite oxide and the reducing agent, where the concentration of the reducing agent is 47-58 wt.% and the mass ratio of the reducing agent to the oxidized graphite is 6-27. The substrate is ground, polished and the mixed solution of the graphite oxide and the reducing agent is evenly coated on the substrate after the cleaning and then kept at a temperature of 50-80 degrees C for 1-4 hours to obtain the foldable graphene film.