• 专利标题:   Preparation of halogenated graphite for use in preparation of halogenated graphene, involves reacting expanded graphite with halogen simple substance under microwave radiation.
  • 专利号:   CN101920954-A, CN101920954-B
  • 发明人:   ZHENG J, LIU H, LIU Y, ZHU D, WU B, YU G, DI Z, GUO Y
  • 专利权人:   CHINESE ACAD SCI INST CHEM, CHINESE ACAD SCI CHEM INST
  • 国际专利分类:   C01B031/00
  • 专利详细信息:   CN101920954-A 22 Dec 2010 C01B-031/00 201128 Pages: 12 Chinese
  • 申请详细信息:   CN101920954-A CN10244635 03 Aug 2010
  • 优先权号:   CN10244635

▎ 摘  要

NOVELTY - Halogenated graphite is obtained by reacting expanded graphite with a halogen simple substance under microwave radiation. USE - Preparation of halogenated graphite for use in preparation of halogenated graphene (all claimed). ADVANTAGE - The method enables simple, quick and economical large-scale preparation of halogenated graphite and halogenated graphene with high yield. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for the following: (1) halogenated graphite; (2) preparation of halogenated graphene, which involves dispersing and centrifuging halogenated graphite, and collecting supernatant; and (3) halogenated graphene comprising halogen and graphite bonded by carbon-halogen covalent bond. The content of halogen in the halogenated graphene is 0.5-4 wt.%. The halogen is bromine or chlorine.