• 专利标题:   Preparation of anode material for polyanionic sodium battery based on organic acid dissolution method, involves preparing mixture of transition metal source and polyanion source, and further adding carbon source, stirring, drying to obtain precursor powder, heat treating and cooling.
  • 专利号:   CN113745506-A, CN113745506-B, WO2023024769-A1
  • 发明人:   YANG H, AI X, ZHAO A, CAO Y
  • 专利权人:   UNIV WUHAN, SHENZHEN JIANA ENERGY TECHNOLOGY CO LTD, SHENZHEN JANAENERGY TECHNOLOGY CO LTD
  • 国际专利分类:   H01M010/054, H01M004/58, H01M004/587
  • 专利详细信息:   CN113745506-A 03 Dec 2021 H01M-004/58 202229 Chinese
  • 申请详细信息:   CN113745506-A CN10992430 27 Aug 2021
  • 优先权号:   CN10992430

▎ 摘  要

NOVELTY - Preparation of anode material, involves (S1) preparing mixture of transition metal source, sodium source and polyanion source and adding it to a reactor, where the transition metal source is simple transition metal or transition metal oxide, (S2) adding organic acid to the reactor, heating, and stirring continuously until the transition metal source is completely dissolved, (S3) adding carbon source, stirring and drying to obtain precursor powder, (S4) subjecting the precursor powder to heat treatment in an inert gas atmosphere, and cooling to room temperature with a furnace after the heat treatment is completed. USE - Preparation of anode material for polyanionic sodium battery based on organic acid dissolution method. ADVANTAGE - The mixed solution has uniform ion distribution, and the dried precursor particles are small, and the corresponding electrode material can be directly calcined at high temperature without the need for crushing treatment.