• 专利标题:   Producing green emitting graphene quantum dots from coal, involves chemically oxidizing coal in acidic environment, filtering coal through PTFE membrane, hydrothermally cutting coal, and purifying coal by Whatman filter paper technique.
  • 专利号:   IN201831004998-A
  • 发明人:   GHORAI S, DASH P S, ROY I, CHATTOPADHYAY D
  • 专利权人:   TATA STEEL LTD, DEPT POLYMER SCI TECHNOLOGY
  • 国际专利分类:   C09K011/00
  • 专利详细信息:   IN201831004998-A 16 Aug 2019 C09K-011/00 201972 Pages: 15 English
  • 申请详细信息:   IN201831004998-A IN31004998 09 Feb 2018
  • 优先权号:   IN31004998

▎ 摘  要

NOVELTY - Method for producing green emitting graphene quantum dots from coal, involves chemically oxidizing coal in an acidic environment, filtering the oxidizing coal in neutral pH through a PTFE membrane and retaining the size of 0.45 mm, hydrothermally cutting the oxidized coal at 120-130 degrees C for 2-3 hours, and purifying the oxidized coal by Whatman filter paper technique. USE - The method is useful for producing green emitting graphene quantum dots from coal. ADVANTAGE - The method: utilizes cheap and abundantly available precursor material (coal); allows for direct and rapid (12 hours) synthesis, and very simple separation step; utilizes innovative hydrothermal process (pressure cooker/autoclave treatment) which occurs at low temperature (130 degrees C); and provides moderately high (45%) product yield. The produced green quantum dots exhibit green fluorescent property of 3.5%, quantum yield efficiency with uniform distribution of particle size (4-8 nm). DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the graphene quantum dots having functional groups in combinations of carboxylic acid, epoxy, alkoxy and hydroxyl groups on their aromatic surfaces.