• 专利标题:   Preparing nitrogen-doped reduced graphene oxide supported manganese nanoparticle catalyst comprises e.g. dispersing graphene oxide in alcohol-water mixed solvent, adding polyethylene glycol, water-soluble manganese salt and organic nitrogen source, hydrothermally reacting and drying.
  • 专利号:   CN114976062-A
  • 发明人:   ZHAO Y, YANG X, LIU K, XU M
  • 专利权人:   UNIV KUNMING SCI TECHNOLOGY
  • 国际专利分类:   B82Y040/00, H01M004/90
  • 专利详细信息:   CN114976062-A 30 Aug 2022 H01M-004/90 202288 Chinese
  • 申请详细信息:   CN114976062-A CN11102127 15 Oct 2020
  • 优先权号:   CN11102127

▎ 摘  要

NOVELTY - Preparing nitrogen-doped reduced graphene oxide supported manganese nanoparticle catalyst comprises (i) dispersing graphene oxide in an alcohol-water mixed solvent to obtain a graphene oxide suspension; (ii) adding polyethylene glycol, water-soluble manganese salt and organic nitrogen source to the graphene oxide suspension, and adjusting the pH of the resulting mixed solution to alkaline; (iii) placing the mixed solution in an autoclave, cooling, washing, hydrothermally reacting, and drying to obtain a solid mixture of nano-manganese oxide precursor and nitrogen-doped reduced graphene oxide; and (iv) heat treating solid mixture in an inert atmosphere of 800-1200℃ for a predetermined time. The manganese salt is manganese acetate, and the organic nitrogen source is dimeric cyanamide. USE - The method is useful for preparing nitrogen-doped reduced graphene oxide supported manganese nanoparticle catalyst. ADVANTAGE - The catalyst has good catalytic activity, stability and methanol resistance. DESCRIPTION OF DRAWING(S) - The diagram shows a flowchart of the method for preparing nitrogen-doped reduced graphene oxide supported manganese nanoparticle catalyst (Drawing includes non-English language text).