• 专利标题:   Preparing platinum-carbon catalyst involves adding chloroplatinic acid hexahydrate, carbon material, polyol and protective agent in water, stirring, and alkali to adjust pH value to obtain mixture, pumping it into microchannel reactor for reaction, washing, filtering, and drying.
  • 专利号:   CN113555567-A
  • 发明人:   CHEN J, ZHANG Y, LIU K, LIU Q, BAO Z
  • 专利权人:   WUXI WEIFU HIGHTECHNOLOGY GROUP CO LTD
  • 国际专利分类:   H01M004/92, H01M004/88
  • 专利详细信息:   CN113555567-A 26 Oct 2021 H01M-004/88 202102 Chinese
  • 申请详细信息:   CN113555567-A CN10831034 22 Jul 2021
  • 优先权号:   CN10831034

▎ 摘  要

NOVELTY - Preparation method of platinum-carbon catalyst, involves (a) preparing a mixed solution by adding 4-6 pts. wt. chloroplatinic acid hexahydrate, 1.1-1.4 pt. wt. carbon material, polyol and 10-55 pts. wt. protective agent to 100 pts. wt. water, uniformly stirring, adding an alkali to adjust the pH value to obtain a mixture with a pH value of 6-12, (b) pumping the mixture into the microchannel reactor for reaction through a pump to obtain a reaction product, and (c) washing the reaction product with ultrapure water, filtering under pressure to obtain a filter residue and a filtrate, and drying the filter residue in an oven to obtain a platinum-carbon catalyst. USE - The method is used for preparation of platinum-carbon catalyst (claimed) used in proton exchange membrane fuel cell (PEMFC) used in automobile. ADVANTAGE - The method provides a high speed and high efficiency, low cost, technique environmentally-friendly synthesis method of platinum-carbon catalyst, and has large electrochemical active area and high stability. The method mainly uses water as solvent, avoids the problem caused by safety a large amount of alcohol solvent, and reduces the cost. The method carries out solid-liquid phase reaction in the microchannel reactor, greatly improves the efficiency of mass transfer heat transfer and improves the reaction efficiency.