• 专利标题:   Preparation of casting mold silicone rubber composite material, involves adding nano-ferroferric oxide and nano-fluorinated graphene to solution of polyethylene glycol-400, dissolving in water and ultrasonically dispersing.
  • 专利号:   CN107286661-A
  • 发明人:   WANG H
  • 专利权人:   DONGGUAN JIAQIAN NEW MATERIAL TECHNOLOGY
  • 国际专利分类:   C08K013/06, C08K003/04, C08K003/22, C08K003/26, C08K009/04, C08K009/06, C08L083/04, C08L083/07
  • 专利详细信息:   CN107286661-A 24 Oct 2017 C08L-083/04 201783 Pages: 7 Chinese
  • 申请详细信息:   CN107286661-A CN10469801 20 Jun 2017
  • 优先权号:   CN10469801

▎ 摘  要

NOVELTY - Preparation of casting mold silicone rubber composite material, involves (i) adding nano-ferroferric oxide and nano-fluorinated graphene to solution of polyethylene glycol-400, dissolving in water, ultrasonically dispersing, heating, dripping hexamethyldisilazane, continuously dispersing, maintaining, centrifuging, rinsing and drying to obtain surface-treated nano-particles, (ii) mixing hydrotalcite and surface-treated nano-particles, stirring, dripping silane coupling agent solution, continually mixing, reducing temperature and drying to obtain modified mixed particles. USE - Preparation of casting mold silicone rubber composite material (claimed). ADVANTAGE - The silicone rubber composite material has excellent thermal conductivity, and can maintain good stability at higher temperatures. DETAILED DESCRIPTION - Preparation of casting mold silicone rubber composite material, involves (i) adding nano-ferroferric oxide and nano-fluorinated graphene to a solution of polyethylene glycol-400, dissolving in water, ultrasonically dispersing for 2-3 hours, heating at 40-50 degrees C, dripping hexamethyldisilazane to the mixture, continuously dispersing using a high shear mixer for 1-2 hours, maintaining for 2-3 hours, centrifuging, rinsing, and drying to obtain surface-treated nano-particles, (ii) adding hydrotalcite and surface-treated nano-particles into a high-speed mixer, increasing the temperature to 90 degrees C, stirring at 200-300 rpm, dripping silane coupling agent solution, continually mixing for 30-45 minutes, reducing the temperature to room temperature and drying at 60-80 degrees C to obtain modified mixed particles, (iii) adding silicone rubber and vinyl silicone rubber to a two-roll mixing machine, mixing for 20 minutes, adding modified mixed particles to a mixer, mixing, filtering, adding crosslinking agent, catalyst and curing agent, continually slicing and mixing for 1-2 hours, performing defoaming treatment, adding the mixture into a mold, heating and curing to obtain casting mold silicone rubber composite.