• 专利标题:   Preparation of copper-molybdate-graphene composite material used as cathode material, involves preparing copper molybdate nanoparticles, mixing in graphene oxide aqueous solution, drying and calcining in argon atmosphere.
  • 专利号:   CN106941159-A, CN106941159-B
  • 发明人:   ZHANG L, HE W, GUO S
  • 专利权人:   UNIV SHAANXI SCI TECHNOLOGY, UNIV SHAANXI SCI TECHNOLOGY
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/485, H01M004/587, H01M004/62
  • 专利详细信息:   CN106941159-A 11 Jul 2017 H01M-004/36 201760 Pages: 8 Chinese
  • 申请详细信息:   CN106941159-A CN10175147 22 Mar 2017
  • 优先权号:   CN10175147

▎ 摘  要

NOVELTY - Preparation of copper molybdate-graphene composite material involves dissolving ammonium molybdate tetrahydrate and copper acetate dihydrate in 0.001-0.005 mol/l sodium hydroxide aqueous solution, in the mol ratio of 1-3:1, hydrothermally reacting, centrifuging, washing and drying to obtain ammonium molybdate-copper nanoparticles, preparing 0.5-1 mol/l graphene oxide aqueous solution, adding the nanoparticles, ultrasonically processing the mixture, distilling the product, drying, and calcining the obtained product in argon gas atmosphere. USE - Preparation of copper-molybdate-graphene composite material used as cathode material of lithium ion battery (all claimed). ADVANTAGE - The method produces composite material capable of providing batteries having initial coulombic efficiency of 94%, coulombic efficiency of 99%, reversible specific gravity of 800 mAh/g or more, and charging/discharging cycle time of 64 times or more. The preparation is simple, and carried out using easily available raw materials.