• 专利标题:   Preparation of three-dimensional graphene macroscopic material involves dissolving graphene oxide in organic solution, carrying out solvothermal reaction of mixture of graphene oxide organic solution, cleaning and freezing.
  • 专利号:   CN112537767-A
  • 发明人:   HUANG F, LIU Z, JIN H, SUN T
  • 专利权人:   CHINESE ACAD SCI SHANGHAI CERAMICS INST, SHANGHAI INST CERAMICS CHINESE ACAD SCI
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN112537767-A 23 Mar 2021 C01B-032/184 202138 Pages: 11 Chinese
  • 申请详细信息:   CN112537767-A CN10900128 23 Sep 2019
  • 优先权号:   CN10900128

▎ 摘  要

NOVELTY - Preparation of three-dimensional graphene macroscopic material involves dissolving graphene oxide powder in organic solution to obtain graphene oxide organic solution (A), placing the reaction solution (A) in a reaction kettle, reacting at 100-400 degrees C for 0.5-12 hours by solvothermal method, cleaning and drying. The drying is freezing at -18 degrees C to -30 degrees C and drying at 80-120 degrees C. USE - Preparation of three-dimensional graphene macroscopic material (claimed).