• 专利标题:   Manufacture of graphene-titanium dioxide composite material involves dissolving titanium iron-containing precursor in absolute ethyl alcohol, adding oxidized graphene solution, hydrolyzing, adding aqueous solution, and crystallizing.
  • 专利号:   CN103337611-A, CN103337611-B
  • 发明人:   CHEN H, LI Y, LI X, SONG Z, ZHOU H
  • 专利权人:   UNIV XIAMEN
  • 国际专利分类:   C01B031/04, C01G023/053, H01M004/36
  • 专利详细信息:   CN103337611-A 02 Oct 2013 H01M-004/36 201410 Pages: 9 Chinese
  • 申请详细信息:   CN103337611-A CN10287749 10 Jul 2013
  • 优先权号:   CN10287749

▎ 摘  要

NOVELTY - Manufacture of graphene-titanium dioxide composite material involves preparing solution by dissolving titanium iron-containing precursor in absolute ethyl alcohol, adding oxidized graphene solution, hydrolyzing, obtaining amorphous titanium hydroxide nano-particles, precipitating, drying, obtaining oxidized graphene-titanium oxide composite material, adding an aqueous solution to hydrothermal reaction vessel, adding oxidized graphene-amorphous titanium oxide composite material to aqueous solution, reducing oxidized graphene, and crystallizing amorphous titanium oxide. USE - Manufacture of graphene-titanium dioxide composite material (claimed). ADVANTAGE - The method enables efficient manufacture of graphene-titanium dioxide composite material by an environmentally-friendly process. DETAILED DESCRIPTION - Manufacture of graphene-titanium dioxide composite material involves preparing a solution by dissolving a titanium iron-containing precursor in absolute ethyl alcohol, adding oxidized graphene solution such that titanium irons are adsorbed by the surface of oxidized graphene, hydrolyzing, obtaining amorphous titanium hydroxide nano-particles, precipitating, drying, obtaining oxidized graphene-titanium oxide composite material, adding an aqueous solution into a sealed high-pressure hydrothermal reaction vessel, adding the obtained oxidized graphene-amorphous titanium oxide composite material to the aqueous solution, reducing oxidized graphene, and crystallizing amorphous titanium oxide.