• 专利标题:   Preparing nitrogen-doped graphene using shock wave treated carbonate comprises mixing carbon source, reducing agent and nitrogen source, compacting, flyer plate impact induced chemical reaction with nitric acid, filtering and drying.
  • 专利号:   CN104261388-A, CN104261388-B
  • 发明人:   CHEN P, GAO X, XU C, YIN H, ZHOU Q
  • 专利权人:   BEIJING INST TECHNOLOGY
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104261388-A 07 Jan 2015 C01B-031/04 201515 Pages: 16 Chinese
  • 申请详细信息:   CN104261388-A CN10474600 17 Sep 2014
  • 优先权号:   CN10474600

▎ 摘  要

NOVELTY - Preparing nitrogen-doped graphene using shock wave treated carbonate comprises (a) uniformly mixing carbon source, reducing agent and nitrogen source to obtain powder 1, transferring the powder 1 into a sample box and compacting to obtain a blank having compaction degree of 80-95%, (b) using flyer plate impact sample box induced chemical reaction to obtain powder 2, and (c) transferring powder 2 into a reactor, adding concentrated nitric acid, reacting at 65-80 degrees C for 12-15 hours, filtering, washing to obtain a solid, drying to obtain powder 3, which is nitrogen doped graphene. USE - The method is useful for preparing nitrogen-doped graphene using shock wave treated carbonate (claimed). ADVANTAGE - The method: provides nitrogen doped graphene with 1-6 layers, which has high nitrogen doping amount, good oxygen reduction catalyst activity; is economical, short, simple and convenient for industrial production; has low demand for production conditions; and is safe.