• 专利标题:   Making zero dimensional graphene quantum dots used in e.g. sensing, comprises placing graphite oxide in furnace, flushing furnace with inert gas, introducing hydrogen into furnace, heating graphite oxide in presence of hydrogen and cooling.
  • 专利号:   WO2015022661-A2, WO2015022661-A3, CN105452163-A, US2016207775-A1, CN105452163-B, US9926202-B2
  • 发明人:   SUNDARA R, BABY T T, KANIYOOR A
  • 专利权人:   INDIAN INST TECHNOLOGY MADRAS, INDIAN INST TECHNOLOGY MADRAS
  • 国际专利分类:   A61K049/00, C01B031/04, C09K011/65, C01B032/184, B82Y020/00, B82Y030/00, B82Y040/00, C01B032/16, C01B032/192, C01B032/194
  • 专利详细信息:   WO2015022661-A2 19 Feb 2015 A61K-049/00 201515 Pages: 41 English
  • 申请详细信息:   WO2015022661-A2 WOIB063909 14 Aug 2014
  • 优先权号:   INCH03641

▎ 摘  要

NOVELTY - Making-1 zero dimensional graphene quantum dots (0-D GQDs), comprises: placing graphite oxide (GO) in a furnace; flushing the furnace with an inert gas; introducing hydrogen into the furnace; heating the GO at 200 degrees C in the presence of hydrogen; and cooling the furnace to room temperature. USE - The process is useful for producing 0-D GQDs, which are useful: in biological applications e.g. image scanning and sensing, drug delivery and cancer treatment; and for photovoltaic applications. No biological data given. ADVANTAGE - The process: provides 0-D GQDs, which are water soluble, emit blue light upon exposure to UV light, are biocompatible and have average particle size of 2.2 plus minus 1 nm (all claimed), which is less than any of the 0-D GQDs produced using existing processes; provides 0-D GQDs with uniform size; is easy to handle and fast; and is cost effective. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are also included for: (1) making-2 0-D GQDs, comprising providing a composition comprising dried GO and treating the GO with focused solar radiation; (2) making-3 of 0-D GQDs, comprising drying GO and heating dried GO to 200 degrees C under reduced pressure; (3) making-4 of a composite of 0-D GQD and one dimensional carbon nanotubes (1-D CNT), comprising placing mixture of GO and manganese trinickel (MnNi3) in a furnace, flushing the furnace with an inert gas, introducing hydrogen into the furnace, heating the mixture to 200 degrees C in the presence of hydrogen for 5 minutes, heating the mixture to 700 degrees C, introducing acetylene to the furnace and cooling the furnace to room temperature; and (4) a composition comprising 0-D GQDs having average size of 2.2 plus minus 1 nm and the 0-D GQD absorb UV light and emit blue light.