• 专利标题:   Solubilizing graphite, to prepare reduced graphene useful e.g. to prepare capacitor, comprises reducing graphite by metal to obtain graphite intercalation compound, and exposing the compound to solvent to give reduced graphene solution.
  • 专利号:   FR2919856-A1, WO2009056696-A2, WO2009056696-A3, WO2009056696-A4, EP2176164-A2, FR2919856-B1, JP2010535690-W, US2011130494-A1, EP2719662-A1, JP2015013803-A, JP5710968-B2, US9120675-B2, EP2176164-B1, ES2663530-T3
  • 发明人:   PENICAUD A, VALLES C, ALAIN P, CRISTINA V
  • 专利权人:   CNRS CENT NAT RECH SCI, CNRS CENT NAT RECH SCI, CENT NAT RECH SCI, CNRS CENT NAT RECH SCI, CNRS CENT NAT RECH SCI
  • 国际专利分类:   C01B031/04, C01B031/00, B05D001/02, B05D001/18, B82Y030/00, C08K005/3415, C09D001/00, C09K003/00, B82Y040/00, C01B031/02, C01B032/19, C01B032/194, C01B032/20, C01B032/22
  • 专利详细信息:   FR2919856-A1 13 Feb 2009 C01B-031/04 200913 Pages: 42 French
  • 申请详细信息:   FR2919856-A1 FR005803 09 Aug 2007
  • 优先权号:   FR005803

▎ 摘  要

NOVELTY - Solubilizing process of graphite, comprises: reducing graphite by an alkali metal to obtain a graphite intercalation compound; and exposing the graphite intercalation compound to an aprotic polar solvent to give a reduced graphene solution, where the process is carried out under inert atmosphere. USE - The graphene is useful for the preparation of composite materials. The graphene is useful for the preparation of electronic and microelectronic components, preferably capacitor or transistor. The reduced graphene solution is useful for deposition of graphene on a substrate (all claimed). ADVANTAGE - The process is cost effective to solubilize graphite. The process provides reduced graphene solution with large quantity and high purity. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for: (1) graphene obtained, in the step of evaporation of aprotic polar solvent, by the process; (2) reduced graphene solution obtained by the process; (3) use of graphene for the preparation of composite materials; and (4) use of a reduced graphene solution for deposition of graphene on a substrate.