• 专利标题:   Graphene spherical assembly body for use as cathode material of lithium ion battery has sheet layers perpendicular to the spherical orientation of the assembly.
  • 专利号:   CN102807211-A
  • 发明人:   CHEN X, SONG H, WU B
  • 专利权人:   UNIV BEIJING CHEM TECHNOLOGY
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102807211-A 05 Dec 2012 C01B-031/04 201332 Chinese
  • 申请详细信息:   CN102807211-A CN10306939 24 Aug 2012
  • 优先权号:   CN10306939

▎ 摘  要

NOVELTY - A graphene spherical assembly body with 0.1-10 mu m diameter has the graphene sheet layers perpendicular to the spherical orientation of the assembly. The sheet is 1-7 nm thick. USE - A graphene spherical assembly body is used as cathode material of lithium ion battery. ADVANTAGE - The process is simple. The material is of low cost and high purity. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the preparation of the graphene spherical assembly body comprising dissolving the mixture containing iron catalyst, organic phenol and sulfur at 1:2:1-1:2:10 mass ratio, stirring to uniform ultrasonic dispersion in an organic solvent, reacting mixture at 150-250 degrees C for 4-72 hours, charring under an inert atmosphere protection at 600-1200 degrees C for 4-72 hours, soaking carbonized product in hydrochloric acid to remove iron sulfide, filtering, washing, and drying to obtain the product.