• 专利标题:   Preparation of N-doped carbon-based platinum cobalt alloy oxygen reduction catalyst used as electrocatalyst for electrochemical oxygen reduction in proton exchange membrane fuel cell, involves preparing carbon base solution, dispersion of raw materials, and solvothermal reaction.
  • 专利号:   CN114068969-A
  • 发明人:   LIU Y, QIAO Y, XUE X, CHEN H, WANG Q, CHEN Q
  • 专利权人:   INST PROCESS ENG CHINESE ACAD SCI, ZHENGZHOU INST EMERGING IND TECHNOLOGY
  • 国际专利分类:   B82Y030/00, B82Y040/00, H01M004/88, H01M004/90, H01M004/92
  • 专利详细信息:   CN114068969-A 18 Feb 2022 H01M-004/92 202233 Chinese
  • 申请详细信息:   CN114068969-A CN11381091 20 Nov 2021
  • 优先权号:   CN11381091

▎ 摘  要

NOVELTY - Preparation of nitrogen-doped carbon-based platinum-cobalt alloy oxygen reduction catalyst, involves adding a carbon carrier to an organic solvent, stirring at room temperature to obtain a carbon base solution, adding a platinum precursor, a cobalt precursor, a stabilizer, a dispersant, and a surfactant to the carbon base solution, ultrasonically mixing at room temperature, adding the solution to a PTFE-lined reactor, packaging into a stainless steel shell, placing in a blast drying box for solvothermal reaction, cooling, centrifuging, washing, drying, and grinding to obtain the product as a black powder. USE - Preparation of N-doped carbon-based platinum cobalt alloy oxygen reduction catalyst used as electrocatalyst for electrochemical oxygen reduction in proton exchange membrane fuel cell (all claimed). ADVANTAGE - The N-doped carbon-based platinum-cobalt alloy oxygen reduction catalyst has uniform dispersion and stable characteristics, and exhibits excellent oxygen reducing activity under acidic conditions. The method is simple and low in cost, and enables easy batch preparation. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the N-doped carbon-based platinum-cobalt alloy oxygen reduction catalyst having a grain diameter of 2-5 nm and a particle lattice spacing of 0.19 nm.