• 专利标题:   Preparation of graphene by dispersing graphite oxide in deionized water, adding ammonia water, adding hydrazine hydrate, carrying out ultrasonic treatment, oil bath heating, washing product with deionized water, and suction filtering.
  • 专利号:   CN110862080-A
  • 发明人:   ZHI T
  • 专利权人:   ZHI T
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN110862080-A 06 Mar 2020 C01B-032/184 202026 Pages: 3 Chinese
  • 申请详细信息:   CN110862080-A CN10986497 28 Aug 2018
  • 优先权号:   CN10986497

▎ 摘  要

NOVELTY - Preparation of graphene comprises fully cooling PTFE-lined kettle, graphite having 60 meshes, potassium permanganate, and concentrated sulfuric acid to 2 degrees C in a refrigerator; dispersing graphite oxide in deionized water in a three-neck flask, and adding ammonia water under the ultrasonic wave and strong mechanical stirring, where the mass volume ratio of the graphite oxide and water is 1:5 (g:mL); after 1 hour, adding hydrazine hydrate, where the mass volume ratio of the graphite oxide to hydrazine hydrate is 1:2 (g:mL); carrying out ultrasonic treatment and strong stirring for 2 hours, oil bath heating to 98-100 degrees C, and reducing for 24 hours; and washing the resulting black product with deionized water, and suction filtering until the pH value is 7. USE - The method is used for preparing graphene. ADVANTAGE - The method has a simple operation, and can easily control the temperature.