• 专利标题:   Preparation of graphene oxide nanobelt by adding concentrated sulfuric acid and multi-walled nanotubes in three-necked flask, adding potassium permanganate, heating, pouring water, centrifuging, washing with hydrochloric acid and water.
  • 专利号:   CN106744905-A
  • 发明人:   SUN G
  • 专利权人:   QINGDAO ZHIXIN BIOTECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/198
  • 专利详细信息:   CN106744905-A 31 May 2017 C01B-032/198 201747 Pages: 4 Chinese
  • 申请详细信息:   CN106744905-A CN10792187 18 Nov 2015
  • 优先权号:   CN10792187

▎ 摘  要

NOVELTY - Preparation of graphene oxide nanobelt comprises adding 50 ml concentrated sulfuric acid and 0.1 g multi-walled nanotubes in 150 ml three-necked flask, stirring for 2 hours until appearance of homogeneous black solution, slowly adding 0.1-0.5 g potassium permanganate to solution, stirring mixture at room temperature for 1 hour, heating to 70 degrees C for 1 hour, pouring reaction solution into 500 ml deionized water, centrifuging to get precipitates, washing with dilute hydrochloric acid solution and deionized water. USE - Method for preparing graphene oxide nanobelt (claimed). ADVANTAGE - The method is simple. The cutting degree of oxidation of carbon nanotube is easy to adjust.