• 专利标题:   Preparing graphene-loaded spherical metal comprises preparing expanded graphite and adding into plasma auxiliary high energy ball milling, performing ball milling treatment, cooling ball milling mixture and drying centrifugal product.
  • 专利号:   CN112574795-A, CN112574795-B
  • 发明人:   DAI L, LIAO H
  • 专利权人:   UNIV JIMEI
  • 国际专利分类:   C10M125/00, C10N030/06
  • 专利详细信息:   CN112574795-A 30 Mar 2021 C10M-125/00 202143 Pages: 11 Chinese
  • 申请详细信息:   CN112574795-A CN10941802 30 Sep 2019
  • 优先权号:   CN10941802

▎ 摘  要

NOVELTY - Preparing graphene-loaded spherical metal comprises (i) preparing expanded graphite; (ii) using plasma auxiliary high energy ball milling device, using oleic acid as wet milling medium and surface modifying agent, ball milling the mixed metal powder of copper and tin, performing high pressure discharge treatment in the ball milling process, and controlling the pressure in the ball milling tank to 0.01-0.03 Mpa; (iii) adding expanded graphite in the plasma auxiliary high energy ball milling, performing ball milling treatment and high pressure discharge treatment, and controlling the pressure in the ball milling tank to 0.5-0.1 Mpa; and (iv) cooling the ball milling mixture with petroleum ether, performing ultrasonic oscillation, settling, collecting the upper layer liquid for centrifugal processing, drying the centrifugal product to obtain powder i.e. graphene load spherical metal. USE - The method is useful for preparing graphene-loaded spherical metal. ADVANTAGE - The metal improves the anti-friction and anti-wear performance of lubricant, reduces the wear of mechanical parts, repairs the damaged surface of the substrate surface, forms a good film protection on the surface of the substrate, and can be used as an additive for lubricating oil. DETAILED DESCRIPTION - Preparing graphene-loaded spherical metal comprises (i) preparing expanded graphite; (ii) using plasma auxiliary high energy ball milling device, using oleic acid as wet milling medium and surface modifying agent, ball milling the mixed metal powder of copper and tin, and performing high pressure discharge treatment in the ball milling process, where the discharge voltage is 25-28 KV, the ball milling tank is filled with argon gas as discharge gas, and controlling the pressure in the ball milling tank to 0.01 0.03 Mpa; (iii) adding expanded graphite in the plasma auxiliary high energy ball milling, performing ball milling treatment and high pressure discharge treatment, where the discharge voltage is 18-20 KV, the ball milling tank is filled with argon gas as the discharge gas, and controlling the pressure in the ball milling tank to 0.5-0.1 Mpa; and (iv) cooling the ball milling mixture with petroleum ether, performing ultrasonic oscillation, settling, collecting the upper layer liquid for centrifugal processing, drying the centrifugal product to obtain powder i.e. graphene load spherical metal.