• 专利标题:   Preparing rod-shaped titanium dioxide-based composite photocatalytic antibacterial aqueous interior wall paint comprises e.g. preparing precursor solution of titanium dioxide-based composite photocatalytic particles and mixed paint.
  • 专利号:   CN112795223-A
  • 发明人:   ZHAI F, LI L, LUO Y, CHEN X
  • 专利权人:   UNIV CHONGQING ARTS SCI
  • 国际专利分类:   B01J021/06, B01J035/02, B01J035/10, C09D175/04, C09D005/14, C09D007/80
  • 专利详细信息:   CN112795223-A 14 May 2021 C09D-005/14 202148 Pages: 7 Chinese
  • 申请详细信息:   CN112795223-A CN11630387 31 Dec 2020
  • 优先权号:   CN11630387

▎ 摘  要

NOVELTY - Preparing rod-shaped titanium dioxide-based composite photocatalytic antibacterial aqueous interior wall paint comprises e.g. (i) taking the titanium dioxide source, dissolving it in ultrapure water, controlling the precipitation of titanium-ammonia complex, separating the precipitate by, washing the precipitate fully with ultrapure water and absolute ethanol, and drying to obtain the titanium-ammonia complex precipitate, adding 6 mg/ml solution of photocatalytic nano particles to attached to the titanium ammonia complex precipitate, preparing 3-5 mol/liter precursor solution and carrying out ultrasonic vibration for 30 minutes to disperse fully to obtain a precursor solution of titanium dioxide-based composite photocatalytic particles; (ii) stirring composite precursor solution and components of the aqueous interior wall paint sequentially and mechanically and mixing in the reaction kettle to obtain a mixed paint; and (iii) carrying out microwave reaction synthesis of the mixed paint. USE - The method is useful for preparing rod-shaped titanium dioxide-based composite photocatalytic antibacterial aqueous interior wall paint. ADVANTAGE - The method: provides better stability, better dispersibility and less agglomeration photocatalytic particles, larger specific surface area, more active sites, better antibacterial and inactivation; and utilizes titanium dioxide which is non-toxic, economical, suitable forbidden band width and large specific surface area. DETAILED DESCRIPTION - Preparing rod-shaped titanium dioxide-based composite photocatalytic antibacterial aqueous interior wall paint comprises (i) taking the titanium dioxide source, dissolving it in ultrapure water, controlling the precipitation of titanium-ammonia complex by adding aqueous ammonia solution, separating the precipitate by suction filtration, washing the precipitate fully with ultrapure water and absolute ethanol, and drying in a constant temperature drying box to obtain the titanium-ammonia complex precipitate, adding 6 mg/ml solution of photocatalytic nano particles to attached to the titanium ammonia complex precipitate, preparing 3-5 mol/liter precursor solution through ammonia and ultrapure water and carrying out ultrasonic vibration for 30 minutes to disperse fully to obtain a precursor solution of titanium dioxide-based composite photocatalytic particles; (ii) stirring the composite precursor solution and the components of the aqueous interior wall paint sequentially and mechanically and mixing in the reaction kettle to obtain a mixed paint; and (iii) carrying out microwave reaction synthesis of the mixed paint.