• 专利标题:   Plastic filled with carbon fiber-graphene for preparing light-emitting diode, comprises magnesium oxide, boron nitride, polybutylene terephthalate, ethylene-vinyl acetate, glass fiber, dibutyltin dilaurate, and ethyl orthosilicate.
  • 专利号:   CN106589856-A
  • 发明人:   AN D, GUO H, LIU G, RUAN L, XIA J
  • 专利权人:   TONGLING TONGFENG OPTOELECTRONICS TECHNOLOGY CO LTD
  • 国际专利分类:   C08K013/06, C08K003/04, C08K003/22, C08K003/32, C08K003/36, C08K003/38, C08K005/3492, C08K007/06, C08L023/08, C08L029/14, C08L067/02, C09K005/14
  • 专利详细信息:   CN106589856-A 26 Apr 2017 C08L-067/02 201735 Pages: 5 Chinese
  • 申请详细信息:   CN106589856-A CN11224826 27 Dec 2016
  • 优先权号:   CN11224826

▎ 摘  要

NOVELTY - Plastic filled with carbon fiber-graphene comprises 5-8 pts. wt. magnesium oxide, 8-13 pts. wt. boron nitride, 10-25 pts. wt. polybutylene terephthalate (PBT), 5-10 pts. wt. ethylene-vinyl acetate (EVA), 4- 10 pts. wt. glass fiber, 2-5 pts. wt. 107 glue, 1-2 pts. wt. dibutyltin dilaurate, 1-3 pts. wt. ethyl orthosilicate, 3-7 pts. wt. melamine cyanurate, 2-5 pts. wt. zinc borate, 2-6 pts. wt. hypophosphite, 1-2 pts. wt. bamboo charcoal, 2-3 pts. wt. nano-silicon dioxide, 1-2 pts. wt. dihydroxybutyltin chloride, 2-5 pts. wt. graphene oxide, and 4-6 pts. wt. carbon fiber. USE - Plastic filled with carbon fiber-graphene for preparing light-emitting diode (claimed). ADVANTAGE - The Plastic filled with carbon fiber-graphene has high speed insulating plastic. DETAILED DESCRIPTION - Plastic filled with carbon fiber-graphene comprises 5-8 pts. wt. magnesium oxide, 8-13 pts. wt. boron nitride, 10-25 pts. wt. polybutylene terephthalate (PBT), 5-10 pts. wt. ethylene-vinyl acetate (EVA), 4- 10 pts. wt. glass fiber, 2-5 pts. wt. 107 glue, 1-2 pts. wt. dibutyltin dilaurate, 1-3 pts. wt. ethyl orthosilicate, 3-7 pts. wt. melamine cyanurate, 2-5 pts. wt. zinc borate, 2-6 pts. wt. hypophosphite, 1-2 pts. wt. bamboo charcoal, 2-3 pts. wt. nano-silicon dioxide, 1-2 pts. wt. dihydroxybutyltin chloride, 2-5 pts. wt. graphene oxide, 4-6 pts. wt. carbon fiber, 2-4 pts. wt. alumina, 3-5 pts. wt. 1-butyl-3-methylimidazolium hexafluorophosphate, 0.1-0.5 pts. wt. dicumyl peroxide, 1-2 pts. wt. KH550, ethanol, acetone, sodium hydroxide solution, and distilled water amount. An INDEPENDENT CLAIM is included for a method for preparing plastic filled with carbon fiber-graphene, which involves: (A) mixing KH550 and ethanol, and subjecting into water bath at 70-90 degrees C to obtain mixture; (B) adding obtained mixture into magnesium oxide and boron nitride, and subjecting under stirring condition for 10-30 minutes, and transfer into a straw to the upper solution at 75-95 degrees C to obtain composite; (C) adding melamine cyanurate, sodium hydroxide solution, zinc borate, into obtained composite and subjecting under stirring condition at 65-95 for 1-3 hours to obtain white viscous product; (D) filtering the obtained white viscous product and drying, and mixing with aluminum phosphate, bamboo charcoal at 100-150 degrees C for 1-2 hours, and subjecting under superfine grinding system to obtain composite flame retardant; (E) heating PBT at 150-170 degrees C and mixing with dihydroxybutyltin chloride and subjecting under polymerization for 1-2 hours, and transfer to an ice-water bath, and drying at 105-130 degrees C for 2-4 hours to obtain polymerized mixture; (F) subjecting obtained polymerized mixture under ultrasonic oscillation by adding graphene oxide, carbon fiber and acetone for 1-2 hours to obtain treated solution; (G) drying EVA, alumina and 1-butyl-3-methylimidazolium hexafluorophosphate in a vacuum oven at 60-80 degrees C for 6-10 h to obtain mixed solution; (H) subjecting obtained mixed solution under dynamic curing for 10-20 minutes, and then adding alumina and 1-butyl-3-methyl imidazole hexafluorophosphate and transfer into melt blending processes for 10-30 minutes to obtain homogeneous mixture; (I) subjecting the obtained homogeneous mixture into a high-speed mixer for 1-2 hours, and transfer into extracting at 200-250 degrees C to obtain granules; and (J) subjecting the obtained granules into molding machine at 235-255 degrees C to obtain desired product.