• 专利标题:   Preparation of nickel ferrite-lesser layer graphite broadband wave absorbing powder material by preparing hydrogen peroxide suspension of carbon material, adding e.g. nickel nitrate hexahydrate, shearing, and hydrothermally reacting.
  • 专利号:   CN114275820-A
  • 发明人:   TANG L, XUE P, YUAN G, XU J, OU W
  • 专利权人:   NANTONG JINSHIDA SPECIAL FABRIC CO LTD
  • 国际专利分类:   C01B032/21, C01B032/225, C01G049/00, C09K003/00, H05K009/00
  • 专利详细信息:   CN114275820-A 05 Apr 2022 C01G-049/00 202250 Chinese
  • 申请详细信息:   CN114275820-A CN10027818 11 Jan 2022
  • 优先权号:   CN10027818

▎ 摘  要

NOVELTY - Preparation of nickel ferrite-lesser layer graphite broadband wave absorbing powder material comprises dispersing carbon material in 30 wt.% 3-5% hydrogen peroxide solution, stirring at 85-95degrees Celsius, naturally cooling to room temperature to obtain hydrogen peroxide suspension of carbon material, adding nickel nitrate hexahydrate, ferric nitrate nonahydrate and urea, adding to high-speed liquid phase shearing device, and shearing to obtain homogeneous shear suspension; and placing in a hydrothermal reactor, reacting at 150-170degrees Celsius for 20-26 hours, cooling to room temperature naturally, centrifuging, ultrasonically cleaning centrifugal product with deionized water repeatedly until neutralized, dispersing into mixed solution of deionized water and ethanol, and drying to 50-70degrees Celsius. The molar ratio of nickel and iron is 3:1. The molar ratio of urea and metal ions is 6.6:1. The molar ratio of metal ions and carbon material is 1:1. USE - The method is for preparation of nickel ferrite-lesser layer graphite broadband wave absorbing powder material ADVANTAGE - The method is simple and easy to prepare large quantities of products. The powder enhances the DurdeLorentz resonance, and has absorption bandwidth covering the S, C and X bands. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a nickel ferrite-lesser layer graphite broadband wave absorbing powder material.