• 专利标题:   Preparing modified nano-cellulose aerogel used in adsorption of cupric and lead ion in wastewater, involves dissolving maleopimaric-based vinyl ketone in solvent, adding nano-cellulose, carboxymethyl chitosan, sodium alginate and graphene oxide, and stirring.
  • 专利号:   CN114534695-A, CN114534695-B
  • 发明人:   GAO H, GUAN Y, GAO W, LI W, ZHOU L, JIANG X
  • 专利权人:   UNIV ANHUI AGRIC
  • 国际专利分类:   B01J020/24, B01J020/28, B01J020/30, C02F001/28, C02F101/20
  • 专利详细信息:   CN114534695-A 27 May 2022 B01J-020/24 202290 Chinese
  • 申请详细信息:   CN114534695-A CN10005614 05 Jan 2022
  • 优先权号:   CN10005614

▎ 摘  要

NOVELTY - Preparing modified nano-cellulose aerogel, involves dissolving maleopimaric acid in a first solvent, adding thionyl chloride for reaction to obtain maleopimaric acyl chloride. The maleopimaric acyl chloride is added into a second solvent, and further added vinyl magnesium bromide, and reacted at 60-80℃ for 2-6 hours to obtain maleopimaric vinyl ketone. The maleopimaric-based vinyl ketone is dissolved in a solvent, sequentially added nano-cellulose, carboxymethyl chitosan, sodium alginate and graphene oxide, and stirred at 50-80℃ to react for 12-36 hours to obtain modified nano-cellulose hydrogel, and freeze-dried the modified nano-cellulose hydrogel to obtain aerogel. USE - Method for preparing modified nano-cellulose aerogel used in the adsorption of cupric ion (Cu2+)and lead ion (Pb2+) in wastewater to analyze it (all claimed). ADVANTAGE - The preparation method of the modified nanocellulose aerogel is simple, and the modified nanocellulose aerogel has excellent performance, where the adsorption capacity of Cu2+reaches 190 mgg-1, and adsorption capacity for Pb2+adsorption reaches 550 mgg-1. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for use of modified nano-cellulose aerogel used in the adsorption of cupric ion (Cu2+)and lead ion (Pb2+) in wastewater, where adsorption capacity of the modified nanocellulose aerogel for Cu2+ is 170-190 mg.g -1, and the amount of adsorption for Pb2+ is 450-550 mg.g-1.