• 专利标题:   Preparing paper-based nickel nanotube-graphene doped bismuth sulfide nanorod, comprises selecting common filter paper or chromatographic paper as paper substrate, mixing graphene and bismuth sulfide suspension, using deionized water and anhydrous ethanol, and drying in oven.
  • 专利号:   CN114772639-A
  • 发明人:   YU J, TAN X, LI L, YIN W, LIANG B, CHEN Y
  • 专利权人:   UNIV JINAN
  • 国际专利分类:   B82Y015/00, B82Y040/00, C01B032/184, C01G029/00, C23C018/32
  • 专利详细信息:   CN114772639-A 22 Jul 2022 C01G-029/00 202291 Chinese
  • 申请详细信息:   CN114772639-A CN10316724 29 Mar 2022
  • 优先权号:   CN10316724

▎ 摘  要

NOVELTY - Preparing paper-based nickel nanotube-graphene doped bismuth sulfide nanorod comprises (i) selecting a common filter paper or a chromatographic paper as a paper substrate, (ii) adding 2.1748 g trimellitic anhydride, 30 wt.% hydrogen peroxide and 200 μl aqueous ammonia into a beaker, and taking out a paper chip deionized water finishing reaction, (iii) removing 200 ml water into the beaker, and adding 0.6 g graphene oxide powder and 1.6 g phenylhydrazine-4-sulfonic acid into the beaker, (iv) removing 25 ml ethylene glycol into the beaker, adding 1.35 g urea and 20 ml distilled water into a mixed solution, and continuously stirring for 30 minutes to obtain uniformly mixed bismuth precursor, and (v) mixing a graphene and a bismuth sulfide suspension in a ratio of 1: 2, using a deionized water and an anhydrous ethanol, washing for 3 times, drying for 12 hours in an oven to finish a preparation of paper-based nickel nanotube-graphene doped bismuth sulfide nanorod. USE - The method is used for preparing paper-based nickel nanotube-graphene doped bismuth sulfide nanorod. ADVANTAGE - The paper-based nickel nanotube-graphene doped bismuth sulfide nano-rod has high photoelectric conversion efficiency, and can be combined with paper chip convenient to carry, easy to be folded and laid a good foundation for the preparation of flexible nano-material sensing platform.