• 专利标题:   Preparing nitrogen-sulfur co-doped graphene porous sheet embedded with iron carbide used to degrade organic pollutant in water involves mixing iron salt and sulfur source in water, adding ethanol, carbonizing, neutralizing and grinding.
  • 专利号:   CN112756007-A
  • 发明人:   CHEN W, HE D, HUANG J, HE H, LEI L, SHEN Y
  • 专利权人:   UNIV CHINA ELECTRONIC SCI TECHNOLOGY
  • 国际专利分类:   B01J027/24, B01J035/02, B01J035/10, C02F001/72, C02F101/30
  • 专利详细信息:   CN112756007-A 07 May 2021 B01J-027/24 202155 Pages: 10 Chinese
  • 申请详细信息:   CN112756007-A CN11319476 23 Nov 2020
  • 优先权号:   CN11319476

▎ 摘  要

NOVELTY - Preparing nitrogen-sulfur co-doped graphene porous sheet embedded with iron carbide comprises (a) adding iron salt and sulfur source into deionized water, stirring uniformly, adding nitrogen source and ethyl alcohol, and stirring uniformly to obtain a suspension, where the mass ratio of iron salt to sulfur source and nitrogen source is (0.3-1):(0.2-2):(2-12), and the mass fraction of iron salt in the suspension is 3.75-12.5%, (b) evaporating the solvent in the suspension, and drying to obtain a precursor, (c) adding the precursor in a tubular furnace, heating to 500 degrees C at a rate of 2-5 degrees C/minute in the presence of nitrogen, and carbonizing for 2-4 hours, and (d) heating to 800 degrees C at the heating rate of 2-5 degrees C/minute in the presence of nitrogen, and carbonizing for 2-5 hours, cooling to room temperature, washing with acid, neutralizing, drying, and grinding. USE - The co-doped graphene porous sheet is useful for degrading organic pollutant in water (claimed). ADVANTAGE - The co-doped graphene sheet improves the recycling of carbon materials in the water bodies, reduces secondary pollution caused by metal leaching, and has excellent removal ability of organic pollutants in water.