• 专利标题:   Three-dimensional graphene/iron oxide magnetic nano-adsorbent preparation, used for adsorbing dye contaminants in water, comprises adding iron trichloride hexahydrate into aqueous dispersion of graphene oxide and adding L-cysteine.
  • 专利号:   CN108905973-A
  • 发明人:   LIANG W, HUANG Y, MA X, LI Y, DONG W, DONG C
  • 专利权人:   UNIV SHANXI
  • 国际专利分类:   B01J020/20, B01J020/28, B01J020/30, C02F001/28, C02F001/48, C02F101/30
  • 专利详细信息:   CN108905973-A 30 Nov 2018 B01J-020/20 201914 Pages: 17 Chinese
  • 申请详细信息:   CN108905973-A CN10812972 23 Jul 2018
  • 优先权号:   CN10812972

▎ 摘  要

NOVELTY - Three-dimensional graphene/iron oxide magnetic nano-adsorbent material is prepared by ultrasonic treating 30-50 mg graphene oxide in deionized water for 20 minutes to obtain graphene oxide dispersion liquid, adding 100-120 mg iron trichloride hexahydrate, ultrasonic dissolving, adding 180-220 mg L-cysteine, adding 1 mL ammonia water to adjust pH, and stirring for 95 hours at 3-4 degrees C to magnetic black precipitate reactant; and cooling to room temperature, separating hysteresis and black precipitate, repeatedly washing with deionized water and absolute ethanol, and freeze-drying for 20-30 hours. USE - Three-dimensional graphene/iron oxide magnetic nanoadsorbing material is used for adsorbing cationic, anionic or neutral dye contaminants in water (claimed). ADVANTAGE - The material has low cost, large specific surface area, rich hydroxyl groups and free carboxyl groups, and good magnetic properties. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the use of the nano-adsorbent material for adsorbing cationic, anionic or neutral dye contaminants in water.