• 专利标题:   Preparing graphene involves taking graphite material as anode material, and mixed solution of acid and hydrogen peroxide as electrolyte, and carrying out electrolytic reaction to realize electrochemical stripping of anode material.
  • 专利号:   CN107235485-A
  • 发明人:   DING G, TIAN S, HE P, YANG S, SUN J, WANG H
  • 专利权人:   SHANGHAI XINCHI ENERGY TECHNOLOGY CO LTD, ZHEJIANG CHINT ELECTRICS CO LTD
  • 国际专利分类:   C01B032/19
  • 专利详细信息:   CN107235485-A 10 Oct 2017 C01B-032/19 201775 Pages: 14 Chinese
  • 申请详细信息:   CN107235485-A CN10169717 23 Mar 2016
  • 优先权号:   CN10169717

▎ 摘  要

NOVELTY - The preparation method of graphene involves: (a) taking graphite material as anode material, and mixed solution of acid and hydrogen peroxide as electrolyte, and carrying out electrolytic reaction to realize electrochemical stripping of anode material; (b) carrying out solid-liquid separation and washing on the electrolyte obtained in step (a) to extract graphene precursor dispersed in electrolyte, drying the extracted graphene precursor to obtain graphene sample; and (c) dissolving the graphene sample in organic solvent. USE - The method is useful for preparing graphene (claimed). ADVANTAGE - The method enables simple and economical preparation of graphene with high purity and quality in an environmentally-friendly manner. DETAILED DESCRIPTION - The preparation method of graphene involves: (a) taking graphite material as anode material, and mixed solution of acid and hydrogen peroxide as electrolyte, and carrying out electrolytic reaction to realize electrochemical stripping of anode material; (b) carrying out solid-liquid separation and washing on the electrolyte obtained in step (a) to extract graphene precursor dispersed in electrolyte, drying the extracted graphene precursor to obtain graphene sample; and (c) dissolving the graphene sample in organic solvent, and carrying out ultrasonic treatment on organic solvent dissolved graphene sample to obtain graphene solution.