• 专利标题:   Preparation of titania-based graphene/lanthanum ion carbon fiber by dissolving graphene and polyacrylonitrile in dimethylformamide, adding lanthanum nitrate, glacial acetic acid and tetra-n-butyl titanate mixed solution, and stirring.
  • 专利号:   CN105921142-A
  • 发明人:   SUN Q, WANG F, ZHANG W, ZHANG X
  • 专利权人:   UNIV NANTONG
  • 国际专利分类:   A01N059/00, A01P001/00, B01J023/10, B01J035/06
  • 专利详细信息:   CN105921142-A 07 Sep 2016 B01J-023/10 201676 Pages: 10 Chinese
  • 申请详细信息:   CN105921142-A CN10333209 18 May 2016
  • 优先权号:   CN10333209

▎ 摘  要

NOVELTY - Preparation of titania-based graphene/lanthanum ion carbon fiber comprises dissolving 0.0007-0.0049 g/mL graphene and 0.08 g/mL polyacrylonitrile in dimethylformamide to obtain graphene/polyacrylonitrile dimethylformamide mixture; and adding 0.0069 g/mL lanthanum nitrate to glacial acetic acid and tetra-n-butyl titanate mixed solution at volume ratio of 4:5, slowly adding into graphene/polyacrylonitrile dimethylformamide mixture at volume ratio of 50:9 while stirring, vacuum stirring to obtain spinning solution, electrospinning, drawing, pre-oxidizing, and calcining. USE - Method for preparation of titania-based graphene/lanthanum ion carbon fiber (claimed). ADVANTAGE - The method has high strength, simple production equipment, simple operation, and good antibacterial effect.