• 专利标题:   Preparing antistatic textile fabric used in the field of medical protective clothing, comprises dissolving tetrabutyl titanate in ethylene glycol and stirring, then adding the catalyst slurry into the terephthalic acid and ethylene glycol, melt-spinning antistatic polyester slice, and blending.
  • 专利号:   CN115874304-A
  • 发明人:   ZHENG W
  • 专利权人:   ZHENG W
  • 国际专利分类:   A41D013/008, A41D013/12, A41D031/26, D01F001/09, D01F001/10, D01F006/92, D04B001/16
  • 专利详细信息:   CN115874304-A 31 Mar 2023 D01F-006/92 202335 Chinese
  • 申请详细信息:   CN115874304-A CN11449554 18 Nov 2022
  • 优先权号:   CN11449554

▎ 摘  要

NOVELTY - Preparing antistatic textile fabric comprises (i) dissolving graphene oxide in water, dispersing to obtain graphene oxide hydrosol, stirring, then filtering, washing and drying to obtain the modified graphene oxide, (ii) dissolving the modified graphene oxide in water, and dispersing, then adding KH-560 and nano-silicon dioxide into the modified graphene oxide hydrosol, stirring, then filtering, washing and drying to obtain a mixture M, (iii) dissolving sodium citrate in water, adding the mixture M, stirring, washing and drying, (iv) mixing and stirring the antistatic agent and ethylene glycol, and dispersing uniformly, (v) dissolving tetrabutyl titanate in ethylene glycol and stirring, then adding the catalyst slurry into the terephthalic acid and ethylene glycol, (vi) adding the antistatic agent slurry into the polymerization raw material, (vii) discharging the material, and (viii) melt-spinning antistatic polyester slice, blending into yarn-static textile fiber. USE - The preparing antistatic textile fabric is used in the field of medical protective clothing (claimed). ADVANTAGE - The textile fabric has good antistatic performance, the anti-static component is not easy to fall off after water washing, and has permanent antistatic property. DETAILED DESCRIPTION - Preparing antistatic textile fabric comprises (i) dissolving graphene oxide in water, ultrasonically dispersing to obtain graphene oxide hydrosol, then adding dodecyltrimethylammonium chloride to graphene oxide hydrosol, stirring at constant temperature, then filtering, washing and drying to obtain the modified graphene oxide, (ii) dissolving the modified graphene oxide in water, and ultrasonically dispersing to obtain the modified graphene oxide hydrosol, then adding KH-560 and nano-silicon dioxide into the modified graphene oxide hydrosol, stirring at constant temperature, then filtering, washing and drying to obtain a mixture M, (iii) dissolving sodium citrate in water, adding the mixture M, stirring at a constant temperature, then filtering, washing and drying to obtain an antistatic agent, (iv) mixing and stirring the antistatic agent and ethylene glycol, and dispersing uniformly to obtain the antistatic agent slurry, (v) dissolving tetrabutyl titanate in ethylene glycol and stirring uniformly to obtain a catalyst slurry, then adding the catalyst slurry into the terephthalic acid and ethylene glycol and stirring uniformly to obtain a polymerization raw material, (vi) adding the antistatic agent slurry into the polymerization raw material, stirring uniformly, and placing into the polyester reaction vessel, (vii) discharging the material, then drying and cutting to obtain antistatic polyester slice, and (viii) melt-spinning antistatic polyester slice, and then forming antistatic fiber through fiber forming, drawing and orientation of primary fiber, heat setting and winding the fiber to obtain antistatic fiber, blending the anti-static fiber into yarn-static textile fiber according to the normal weft knitting weaving process.