• 专利标题:   Transfer of graphene thin film for physical adsorption, involves absorbing polyethylene terephthalate-silica gel on graphene/metal layer, etching metal layer, constructing washed/dried structure on substrate, and lifting off gel layer.
  • 专利号:   CN102795619-A, CN102795619-B
  • 发明人:   CHEN X, LIU Z, TIAN J
  • 专利权人:   UNIV NANKAI
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102795619-A 28 Nov 2012 C01B-031/04 201340 Pages: 7 Chinese
  • 申请详细信息:   CN102795619-A CN10322007 04 Sep 2012
  • 优先权号:   CN10322007

▎ 摘  要

NOVELTY - A glass sheet or other relatively flat structure is used for graphene thin-film processing. A polyethylene terephthalate (PET)-silica gel structure is absorbed on the graphene/metal thin film. The obtained structure is placed in an etching solution and the metal layer is etched to obtain a PET-silica gel/graphene structure. The structure is washed with dilute hydrochloric acid solution and deionized, and dried. The structure is constructed on a substrate, the PET-silica gel layer is lifted off, and graphene is transferred to the substrate. USE - Transfer of graphene thin film for physical adsorption. ADVANTAGE - The method enables simple, quick and efficient transfer of high-quality graphene thin films on large area of both flexible and rigid substrates, without residue generation. Repeated usage of PET-silica gel layer makes the process economical and environmentally-friendly. DETAILED DESCRIPTION - A glass sheet or other relatively flat structure is used for graphene thin-film processing. A polyethylene terephthalate (PET)-silica gel structure is absorbed on the graphene/metal thin film to obtain a PET-silica gel/graphite/metal structure. The obtained structure is placed in an etching solution and the metal layer is etched to obtain a PET-silica gel/graphene structure. The obtained structure is washed with dilute hydrochloric acid solution and deionized, and dried using nitrogen. The structure is constructed on a substrate, the PET-silica gel layer is lifted off, and graphene is transferred to the substrate.