• 专利标题:   Alpha-ferric oxide/nano graphene composite material surface-enhanced Raman scattering substrate and photocatalyst used for decomposing organic matter, comprises alpha-ferric oxide/graphene nanoparticles of quasi-cubic shape.
  • 专利号:   CN104907070-A
  • 发明人:   HU F, LI C, YE X, WU M, YAN T, ZHANG L, SUN J
  • 专利权人:   NINGBO XIBOEN NEW MATERIAL TECHNOLOGY CO
  • 国际专利分类:   A62D003/17, B01J023/745, G01N021/65
  • 专利详细信息:   CN104907070-A 16 Sep 2015 B01J-023/745 201614 Pages: 12 Chinese
  • 申请详细信息:   CN104907070-A CN10169281 09 Apr 2015
  • 优先权号:   CN10169281

▎ 摘  要

NOVELTY - An alpha -ferric oxide/nano graphene composite material surface-enhanced Raman scattering substrate and photocatalystcomprises alpha -ferric oxide/graphene nanoparticles of quasi-cubic shape, with a particle size distribution of 60-80 nm and a graphene size of 10-50 mu m. USE - alpha -Ferric oxide/nano graphene composite material surface-enhanced Raman scattering substrate and photocatalyst (claimed). ADVANTAGE - The alpha -ferric oxide/nano graphene composite material surface-enhanced Raman scattering substrate and photocatalyst has a particle size of less than 100 nm, high capacity, and excellent organic-matter decomposition efficiency, and can be prepared by an economical and safe method. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of alpha -ferric oxide/nano graphene composite material surface-enhanced Raman scattering substrate and photocatalyst, which involves adding iron salt to anhydrous ethanol, magnetically stirring for 10-20 minutes, adding polyvinylpyrrolidone to anhydrous ethanol, magnetically stirring for 10-20 minutes, mixing both solutions, adding distilled water, magnetically stirring for 10-30 minutes, adding aqueous ammonia, magnetically stirring for 10-20 minutes, heating for 12-18 hours at 200 degrees C, centrifugally washing 3-5 times, drying at 60-90 degrees C to obtain quasi-cubic ferric oxide nanoparticles, redissolving in distilled water, magnetically stirring for 10-20 minutes, adding graphene oxide solution, stirring for 20-40 minutes, seal-reacting in 30-100 mL container at 130-200 degrees C for 8-20 hours, naturally cooling to room temperature, and drying at 60-90 degrees C.