• 专利标题:   Preparation of water-soluble graphene includes dispersing graphene oxide in water, adding sulfur-containing phenylhydrazine compound, evaporating mother liquor, and removing sulfur-containing phenylhydrazine compound excess.
  • 专利号:   CN103435031-A, CN103435031-B
  • 发明人:   WANG L, LIU Y, WANG P
  • 专利权人:   UNIV YANSHAN
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103435031-A 11 Dec 2013 C01B-031/04 201415 Pages: 8 Chinese
  • 申请详细信息:   CN103435031-A CN10296390 16 Jul 2013
  • 优先权号:   CN10296390

▎ 摘  要

NOVELTY - Water-soluble graphene is prepared by dispersing graphene oxide in water, adding sulfur-containing phenylhydrazine compound at graphene oxide and sulfur-containing phenylhydrazine compound 1:1-6 mass ratio, ultrasonic washing for l-2 hours, reacting at 70-90 degrees C for 4-18 hours, filtering to remove insoluble impurities, evaporating mother liquor under reduced pressure, concentrating, removing sulfur-containing phenylhydrazine compound excess, and vacuum drying at 60 degrees C. USE - Method for preparing water-soluble graphene (claimed). ADVANTAGE - The graphene has good solubility.