• 专利标题:   Preparing hollow cobalt sulfide/ruthenium nitride composite material with rich sulfur vacancy, comprises e.g. adding oxidation graphene into deionized water, ultrasonically dispersing, adding ascorbic acid and stirring uniformly.
  • 专利号:   CN114613608-A
  • 发明人:   TAO K, TAN S
  • 专利权人:   UNIV NINGBO
  • 国际专利分类:   H01G011/24, H01G011/32, H01G011/86
  • 专利详细信息:   CN114613608-A 10 Jun 2022 H01G-011/32 202264 Chinese
  • 申请详细信息:   CN114613608-A CN10279692 06 Mar 2022
  • 优先权号:   CN10279692

▎ 摘  要

NOVELTY - Preparing hollow cobalt sulfide/red-green (RGO) composite material rich in sulfur vacancy comprises (a) introducing 0.015 g oxidation graphene (GO) to 40 ml deionized water, ultrasonically dispersing for 1 hour, adding 0 1 g ascorbic acid and stirring uniformly, introducing a piece of clean foam nickel under the water bath condition of 80degrees Celsius heating for 6 hours, taking out and washing, dry to obtain RGO/NF; (b) completely dissolving 1.313 g 2-methylimidazole and 0.5820 g nitrate hexahydrate in 40 ml deionization water, mixing the solution, adding RGO /NF, stirring for 10 minutes; (c) placing cobalt sulfide/RGO / NF in 0.5 M sodium tetrahydridoborate solution, soaking for 2 hours at room temperature, washing, and drying. USE - The method is useful for preparing hollow Co3S4/RGO composite material with rich sulphur vacancy, which is useful in super capacitor. ADVANTAGE - The hollow composite material has improved electrochemical performance, conductivity and stability, and improves performance of super capacitor.