• 专利标题:   Preparing graphene thin film, comprises soaking graphene oxide film in ethanol solution, drying to obtain graphene oxide film intercalated with ethanol, subjecting graphene oxide film intercalated with ethanol to thermal annealing treatment, thermal reduction treatment and graphitization.
  • 专利号:   CN115231557-A
  • 发明人:   ZHANG J, SONG M, JIN C
  • 专利权人:   TAICANG SIDIKE NEW MATERIAL TECHNOLOGY, JIANGSU SIDIKE NEW MATERIALS TECHNOLOGY
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN115231557-A 25 Oct 2022 C01B-032/184 202295 Chinese
  • 申请详细信息:   CN115231557-A CN10695504 20 Jun 2022
  • 优先权号:   CN10695504

▎ 摘  要

NOVELTY - Preparing graphene thin film, comprises soaking the graphene oxide film in an ethanol solution, and drying to obtain a graphene oxide film intercalated with ethanol, subjecting the graphene oxide film intercalated with ethanol sequentially to thermal annealing treatment, thermal reduction treatment and graphitization treatment to obtain a graphene film, where the thermal annealing treatment, the thermal reduction treatment and the graphitization treatment adopt pressure sintering, the temperature of the thermal annealing treatment is 100-200℃, the time is 0.5-4 hours, and the applied pressure is 5-30t; the temperature of the thermal reduction treatment is 1100-1500℃, the time is 0.5-4 hours, and the applied pressure is 30-70t; the temperature of the graphitization treatment is 2500-3000℃, the time is 0.5-4 hours, and the applied pressure is 30-70t. USE - The method is useful for preparing film graphene, which is useful in heat management system for transfer of electronic industry and space instrument heat energy, and conversion and storage. ADVANTAGE - The heat-conducting property of the graphene film prepared by the preparation method is good and stable. The method improves the heat conducting performance of the thin film. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a graphene thin film, obtained by the method as mentioned above.