• 专利标题:   Method for improving macroscopic lubricating performance of graphene based on annealing treatment, involves quickly cooling graphene/silicon dioxide sample to about 30 degrees centigrade, and obtaining graphene coating with excellent macroscopic lubricating performance.
  • 专利号:   CN114956064-A
  • 发明人:   QIAN L, YANG L, LIU Y, LIU L, ZHOU X, WEI L, CHEN L
  • 专利权人:   UNIV SOUTHWEST JIAOTONG
  • 国际专利分类:   B05D003/04, C01B032/194
  • 专利详细信息:   CN114956064-A 30 Aug 2022 C01B-032/194 202295 Chinese
  • 申请详细信息:   CN114956064-A CN10498061 07 May 2022
  • 优先权号:   CN10498061

▎ 摘  要

NOVELTY - The method involves mixing (S1) graphene powder, deionized water and surfactant to obtain mixed solution A. The mixed solution A is ultrasonically processed (S2). The mixed solution A is dropped on a silicon dioxide substrate. An annealing treatment is performed (S3) under high purity argon gas after drying. A graphene/silicon dioxide sample is quickly cooled to about 30 degrees centigrade. A graphene coating is obtained (S4) with excellent macroscopic lubricating performance. A granularity of the graphene powder is 0.5 to 20 microns, preferably 3 microns. A surfactant is non-surfactant, preferably isooctyl phenyl polyoxyethylene ether. A mass concentration of the isooctyl phenyl polyoxyethylene ether in the obtained mixed solution A is 0.024 % to 0.25 %, preferably 0.1 %. USE - Method for improving macroscopic lubricating performance of graphene based on annealing treatment used for multi-scale lubricant and lubricating additive. DESCRIPTION OF DRAWING(S) - The drawing shows a flowchart illustrating a method for improving macroscopic lubricating performance of graphene based on annealing treatment. (Drawing includes non-English language text) S1Step for mixing graphene powder, deionized water and surfactant to obtain mixed solution A S2Step for ultrasonically processing mixed solution A S3Step for dropping mixed solution A on silicon dioxide substrate and performig annealing treatment S4Step for quickly cooling graphene/silicon dioxide sample and obtaining graphene coating with excellent macroscopic lubricating performance