• 专利标题:   Method of macro-mass preparation of hydroxyl-rich epoxy-type graphite involves mixing graphite flakes and first sulfuric acid and reacting, and adding second sulfuric acid to cooperate with first sulfuric acid to intercalate and modify graphite flakes to second graphite precursor.
  • 专利号:   CN114590805-A
  • 发明人:   HAO Z, LUO L, LV J, YU Z, CAI J
  • 专利权人:   GUANGDONG MORION NANOTECH CO LTD, KUNMING YUNTIAN MORUI TECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/194, C01B032/198
  • 专利详细信息:   CN114590805-A 07 Jun 2022 C01B-032/198 202292 Chinese
  • 申请详细信息:   CN114590805-A CN10330835 31 Mar 2022
  • 优先权号:   CN10330835

▎ 摘  要

NOVELTY - Method of macro-mass preparation of hydroxyl-rich epoxy-type graphite, involves mixing graphite flakes and first sulfuric acid and reacting to obtain first graphite precursor, and adding second sulfuric acid to cooperate with first sulfuric acid to intercalate and modify the graphite flakes to obtain second graphite precursor, where first sulfuric acid is selected from concentrated sulfuric acid with mass fraction of more than 98%, and the second sulfuric acid is selected from sulfuric acid with mass fraction of 10-90%. USE - Method of macro-mass preparation of hydroxyl-rich epoxy-type graphite. ADVANTAGE - The method is simple and economical. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for hydroxyl-rich epoxy graphene oxide, which has content of carboxyl and carbonyl functional groups less than 2%, and content of hydroxyl and epoxy groups of more than 60%.