• 专利标题:   Preparing coal-based graphene comprises mixing e.g. concentrated phosphoric acid with coal-based graphite, filtering, washing, drying, ultrasonic dispersion, mixing with aqueous ammonia and hydrazine hydrate, separating and drying.
  • 专利号:   CN110015654-A
  • 发明人:   LI J, ZHANG Q, GUO T
  • 专利权人:   ENN INNER MONGOLIA GRAPHENE MATERIALS CO
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN110015654-A 16 Jul 2019 C01B-032/184 201972 Pages: 11 Chinese
  • 申请详细信息:   CN110015654-A CN10019181 09 Jan 2018
  • 优先权号:   CN10019181

▎ 摘  要

NOVELTY - Preparing coal-based graphene comprises (a) mixing concentrated phosphoric acid with coal-based graphite, perchloric acid, concentrated sulfuric acid, water and hydrogen peroxide, filtering, washing and drying to obtain coal-based graphite oxide, (b) adding coal-based graphite oxide to water for carrying out ultrasonic dispersion to obtain coal-based graphene oxide dispersion, and (c) mixing the coal-based graphene oxide dispersion with aqueous ammonia and hydrazine hydrate, separating and drying. USE - The method is useful for preparing coal-based graphene. ADVANTAGE - The method: can achieve large scale production; can improve the preparation method of coal-based graphite oxide; can avoid the issue of excessive cost of graphene products caused by complex coal-based graphene process. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for coal-based graphene prepared by the above method.