• 专利标题:   Preparing modified graphene insulation material involves mixing expanded perlite, polystyrene particles, graphene, ceramic fiber, lecithin and glycerin, adding diphenylsilanediol, refluixng, adding dibutyltin dilaurate, heating, and cooling.
  • 专利号:   CN105174818-A
  • 发明人:   MENG H
  • 专利权人:   MENG H
  • 国际专利分类:   C04B022/02, C04B026/12
  • 专利详细信息:   CN105174818-A 23 Dec 2015 C04B-026/12 201632 Pages: 7 English
  • 申请详细信息:   CN105174818-A CN10573347 10 Sep 2015
  • 优先权号:   CN10573347

▎ 摘  要

NOVELTY - Preparing modified graphene insulation material involves mixing 4-9 pts. wt. expanded perlite, 2-7 pts. wt. polystyrene particles, 1-6 pts. wt. graphene, 3-8 pts. wt. ceramic fiber, 1-5 pts. wt. lecithin, and 3-12 pts. wt. glycerin to obtain a mixture. 10-20 pts. wt. Obtained mixture is heated at 60-80 degrees C, and 3-7 pts. wt. phenol resin and 2-6 pts. wt. diphenylsilanediol are added to obtained mixture under stirring condition to obtain another mixture. Latter mixture is refluxed 8-15 pts. wt. with 20-30 pts. wt. ethanol, and then filtered. Filtered product is dried. USE - Method for preparing modified graphene insulation material. ADVANTAGE - The modified graphene insulation material has flexural strength of more than 10 megapascals, absorption rate below 25%, and thermal conductivity of Watts per meter Kelvin. DETAILED DESCRIPTION - Preparing modified graphene insulation material involves mixing 4-9 pts. wt. expanded perlite, 2-7 pts. wt. polystyrene particles, 1-6 pts. wt. graphene, 3-8 pts. wt. ceramic fiber, 1-5 pts. wt. lecithin, and 3-12 pts. wt. glycerin to obtain a mixture. 10-20 pts. wt. Obtained mixture is heated at 60-80 degrees C, and 3-7 pts. wt. phenol resin and 2-6 pts. wt. diphenylsilanediol are added to obtained mixture under stirring condition to obtain another mixture. Latter mixture is refluxed 8-15 pts. wt. with 20-30 pts. wt. ethanol, and then filtered. Filtered product is dried. 7-20 pts. wt. Dried product is heated under vacuum condition. 1-5 pts. wt. Dibutyltin dilaurate and 3-6 pts. wt. n-butyl borane are added to obtained product under stirring condition, and thne heated at 60-90 degrees C. Obtained product is cooled to room temperature.