• 专利标题:   Preparing graphene comprises dissolving catechol or catechol derivative in solvent to obtain catechol or its derivative solution, grinding graded graphene into powder, mixing with catechol or its derivative solution and stirring.
  • 专利号:   CN106315539-A
  • 发明人:   ZHAO X
  • 专利权人:   RUIYUAN SHANGHAI CHEM CO LTD
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN106315539-A 11 Jan 2017 C01B-031/04 201724 Pages: 6 Chinese
  • 申请详细信息:   CN106315539-A CN10060711 07 Jul 2015
  • 优先权号:   CN10060711

▎ 摘  要

NOVELTY - Preparing graphene comprises: (i) dissolving catechol or catechol derivative in solvent to 0.1 g/ml catechol or its derivative solution; (ii) grinding graded graphene into powder, mixing of graphene powder with catechol or its derivative solution, stirring with magnetic stirrer and dispersing evenly; (iii) carrying out ultrasonically dispersion if step (ii) resultant for 1 hour and transferring into high pressure reactor, placing high pressure reactor in a water bath at 150 degrees C for 14 hours; and (v) filtering the sample, washing, drying under vacuum to obtain graphene. USE - The method is useful for preparing graphene (claimed). ADVANTAGE - The graphene conducting mode to make anode and liquid electrolyte to form a facing point and forms better conductive network. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing graphene-oxide complex comprising: (1) dissolving oxide precursor in the solvent to obtain oxide precursor solution of concentration is 0.2-0.3 g/ml, grinding of graphene into powder; (2) mixing of graphite alkene powder with the oxide precursor solution, stirring, mixing uniformly, dispersing ultrasonically for 1-4 hours, placing the dispersion liquid in high pressure reactor, carrying out hydro-thermal reaction at 150-200 degrees C under water bath for 12-72 hours, filtering the sample, washing with absolute ethyl alcohol, drying under vacuum to obtain graphene-oxide complex.